acide (amino-2 thioxo-2 ethoxy)-imino-2 Z (tritylamino-2 thiazolyl-4)-2 acetique

Base Information

• Chemical Name: acide (amino-2 thioxo-2 ethoxy)-imino-2 Z (tritylamino-2 thiazolyl-4)-2 acetique
• CAS No.: 79728-95-3
• Molecular Formula: C₂₆H₂₂N₄O₃S₂
• Molecular Weight: 502.618
• Mol file: 79728-95-3.mol

Synonyms:acide (amino-2 thioxo-2 ethoxy)-imino-2 Z (tritylamino-2 thiazolyl-4)-2 acetique

Chemical Property of acide (amino-2 thioxo-2 ethoxy)-imino-2 Z (tritylamino-2 thiazolyl-4)-2 acetique

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acide (amino-2 thioxo-2 ethoxy)-imino-2 Z (tritylamino-2 thiazolyl-4)-2 acetique

There total 3 articles about acide (amino-2 thioxo-2 ethoxy)-imino-2 Z (tritylamino-2 thiazolyl-4)-2 acetique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

acide (cyanomethoxy)-imino-2 Z (tritylamino-2 thiazolyl-4)-2 acetique (68672-55-9) → acide (amino-2 thioxo-2 ethoxy)-imino-2 Z (tritylamino-2 thiazolyl-4)-2 acetique (79728-95-3)

Guidance literature:

With hydrogen sulfide; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide; for 0.5h; Ambient temperature;

Reference yield:

2-(2-tritylamino-4-thiazolyl)-2-(cyanomethoxyimino)-acetic acid → acide (amino-2 thioxo-2 ethoxy)-imino-2 Z (tritylamino-2 thiazolyl-4)-2 acetique (79728-95-3)

Guidance literature:

With triethylamine; In N-methyl-acetamide; dichloromethane; water;

Reference yield:

(Z)-2-Hydroxyimino-2-(2-triphenylmethylaminothiazol-4-yl)-acetic acid (68672-45-7) → acide (amino-2 thioxo-2 ethoxy)-imino-2 Z (tritylamino-2 thiazolyl-4)-2 acetique (79728-95-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) potassium carbonate; 2.) sodium hydroxide / 1.) DMF, r.t., 65 h; 2.) dioxane, r.t., 1 h

2: 82 percent / SH₂, triethylamine / dioxane; dimethylformamide / 0.5 h / Ambient temperature

With sodium hydroxide; hydrogen sulfide; potassium carbonate; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;

upstream raw materials:

acide (cyanomethoxy)-imino-2 Z (tritylamino-2 thiazolyl-4)-2 acetique

(Z)-2-Hydroxyimino-2-(2-triphenylmethylaminothiazol-4-yl)-acetic acid