2-[1-(2,6-dimethoxy-4-pentylphenyl)allyl]-5-methyl-5-hexenoic acid methyl ester

Base Information

Chemical Name:2-[1-(2,6-dimethoxy-4-pentylphenyl)allyl]-5-methyl-5-hexenoic acid methyl ester
CAS No.:930598-01-9
Molecular Formula:C₂₄H₃₆O₄
Molecular Weight:388.547
Hs Code.:

Synonyms:2-[1-(2,6-dimethoxy-4-pentylphenyl)allyl]-5-methyl-5-hexenoic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[1-(2,6-dimethoxy-4-pentylphenyl)allyl]-5-methyl-5-hexenoic acid methyl ester

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Technology Process of 2-[1-(2,6-dimethoxy-4-pentylphenyl)allyl]-5-methyl-5-hexenoic acid methyl ester

There total 3 articles about 2-[1-(2,6-dimethoxy-4-pentylphenyl)allyl]-5-methyl-5-hexenoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 930598-00-8
3-(2,6-dimethoxy-4-pentyl-phenyl)-pent-4-enoic acid methyl ester

: 154106-15-7
3-methylbut-3-en-1-yl trifluoromethanesulphonate

: 930598-01-9
2-[1-(2,6-dimethoxy-4-pentylphenyl)allyl]-5-methyl-5-hexenoic acid methyl ester

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -40 ℃;
DOI:10.1021/ol063022k

Reference yield:

: 930597-96-9
dimethyl [1-(2,6-dimethoxy-4-pentylphenyl)allyl]malonate

: 930598-01-9
2-[1-(2,6-dimethoxy-4-pentylphenyl)allyl]-5-methyl-5-hexenoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / aq. NaCl / dimethylsulfoxide / 160 °C

2: 50 percent / LiHMDS / tetrahydrofuran / -40 °C

With sodium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; dimethyl sulfoxide; 1: Krapcho decarboxylation;
DOI:10.1021/ol063022k