(S)-4-methyl-1-piperazine

Base Information

Chemical Name:(S)-4-methyl-1-piperazine
CAS No.:100158-67-6
Molecular Formula:C₁₈H₂₅N₃O₃
Molecular Weight:331.415
Hs Code.:

(S)-4-methyl-1-<N-(benzyloxycarbonyl)prolyl>piperazine

Synonyms:(S)-4-methyl-1-piperazine

Suppliers and Price of (S)-4-methyl-1-piperazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-4-methyl-1-piperazine

Chemical Property:

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Technology Process of (S)-4-methyl-1-piperazine

There total 1 articles about (S)-4-methyl-1-piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 109-01-3
1-methyl-piperazine

: 1148-11-4
N-Benzyloxycarbonyl-L-proline

: 100158-67-6
(S)-4-methyl-1-piperazine

Guidance literature:: 1-methyl-piperazine; N-Benzyloxycarbonyl-L-proline; With dmap; In dichloromethane; at 0 ℃; for 0.0833333h;

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 24h;

Reference yield: 90.0%

: 100158-67-6
(S)-4-methyl-1-piperazine

: 100158-68-7,116818-82-7
(4-Methyl-piperazin-1-yl)-(S)-pyrrolidin-2-yl-methanone

Guidance literature:: With palladium on activated charcoal; hydrogen; In methanol; at 20 ℃; for 24h; under 760.051 Torr;

Reference yield:

: 100158-67-6
(S)-4-methyl-1-piperazine

: 91790-92-0
(S)-2-<(4-methyl-1-piperazinyl)methyl>pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 5percent Pd/C / methanol

2: LiAlH₄ / tetrahydrofuran / 20 h / Heating

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1246/bcsj.63.721