Technology Process of C15H13N3O2
There total 2 articles about C15H13N3O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium hydroxide / ethanol / 12 h / 120 °C / Sealed tube
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide;
In
ethanol; dichloromethane;
DOI:10.1021/acs.orglett.0c01469
- Guidance literature:
-
Multi-step reaction with 3 steps
1: silver(l) oxide; potassium pivalate; potassium hydrogencarbonate; copper(II) dipivaloate / dimethyl sulfoxide / 12 h / 45 °C / Schlenk technique; Sealed tube; Inert atmosphere
2: potassium hydroxide / ethanol / 12 h / 120 °C / Sealed tube
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere
With
dmap; copper(II) dipivaloate; potassium pivalate; potassium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; silver(l) oxide;
In
ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/acs.orglett.0c01469
- Guidance literature:
-
With
copper diacetate; sodium carbonate;
at 80 ℃;
for 6h;
regioselective reaction;
Sealed tube;
DOI:10.1021/acs.jafc.9b05349
