C₂₅H₃₆BrClN₂O₅

Base Information

Chemical Name:C₂₅H₃₆BrClN₂O₅
CAS No.:1009094-13-6
Molecular Formula:C₂₅H₃₆BrClN₂O₅
Molecular Weight:559.928
Hs Code.:

C<sub>25</sub>H<sub>36</sub>BrClN<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₅H₃₆BrClN₂O₅

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Chemical Property of C₂₅H₃₆BrClN₂O₅

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Technology Process of C₂₅H₃₆BrClN₂O₅

There total 9 articles about C₂₅H₃₆BrClN₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1009094-12-5
C₁₅H₁₇BrClNO₅

: 13293-47-5
(1S,2S,3S,5R)-(+)-isopinocampheylamine

: 1009094-13-6
C₂₅H₃₆BrClN₂O₅

Guidance literature:: (1S,2S,3S,5R)-(+)-isopinocampheylamine; With trimethylaluminum; In hexane; dichloromethane; at 20 ℃; for 1h;

C₁₅H₁₇BrClNO₅; In hexane; dichloromethane; at 20 ℃; for 12h;

With Rochelle's salt; In hexane; dichloromethane; water; at 20 ℃; for 2h;

Reference yield:

: 1009094-06-7
3-bromo-6-chloro-2-hydroxybenzaldehyde

: 1009094-13-6
C₂₅H₃₆BrClN₂O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C

1.2: 20 °C

2.1: sodium hydroxide; hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 1 h / 20 °C / pH 9

3.1: hydrogenchloride; sodium cyanoborohydride; methyl red / tetrahydrofuran; methanol; water / 12 h / pH 3

3.2: pH 9

4.1: calcium chloride / diethyl ether / 3 h / 20 °C

5.1: titanium(IV) isopropylate / tetrahydrofuran / 0.25 h / 140 °C / Microwave irradiation

5.2: 20 °C

6.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C

7.1: trimethylaluminum / hexane; dichloromethane / 1 h / 20 °C

7.2: 12 h / 20 °C

7.3: 2 h / 20 °C

With titanium(IV) isopropylate; hydrogenchloride; sodium hydroxide; hydroxylamine hydrochloride; trimethylaluminum; sodium cyanoborohydride; potassium carbonate; methyl red; calcium chloride; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 174913-09-8
2-bromo-5-chloroanisole

: 1009094-13-6
C₂₅H₃₆BrClN₂O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: boron tribromide / dichloromethane / 12.33 h / -40 - 20 °C

2.1: triethylamine; magnesium chloride / tetrahydrofuran / 0.25 h / 160 °C / Microwave irradiation

2.2: 2 h / Heating / reflux

3.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C

3.2: 20 °C

4.1: sodium hydroxide; hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 1 h / 20 °C / pH 9

5.1: hydrogenchloride; sodium cyanoborohydride; methyl red / tetrahydrofuran; methanol; water / 12 h / pH 3

5.2: pH 9

6.1: calcium chloride / diethyl ether / 3 h / 20 °C

7.1: titanium(IV) isopropylate / tetrahydrofuran / 0.25 h / 140 °C / Microwave irradiation

7.2: 20 °C

8.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C

9.1: trimethylaluminum / hexane; dichloromethane / 1 h / 20 °C

9.2: 12 h / 20 °C

9.3: 2 h / 20 °C

With titanium(IV) isopropylate; hydrogenchloride; sodium hydroxide; hydroxylamine hydrochloride; trimethylaluminum; boron tribromide; sodium cyanoborohydride; potassium carbonate; triethylamine; methyl red; calcium chloride; magnesium chloride; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide;