Technology Process of (E)-7-(2-Aminophenoxy)hept-5-enol
There total 8 articles about (E)-7-(2-Aminophenoxy)hept-5-enol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper acetylacetonate; sodium tetrahydroborate;
In
ethanol;
for 1.5h;
DOI:10.1039/cc9960000737
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 86 percent / imidazole / dimethylformamide / 5 h
2: 1.) Me2SO, ClCOCOCl, 2.) Et3N
3: 92 percent / NaH / tetrahydrofuran / 20 h
4: 89 percent / DIBAL-H / benzene / 0.33 h / -70 °C
5: 94 percent / Ph3P, DEAD / tetrahydrofuran
6: 96 percent / TBAF / tetrahydrofuran / 1 h
7: 96 percent / NaBH4, Cu(acac)2 / ethanol / 1.5 h
With
1H-imidazole; copper acetylacetonate; sodium tetrahydroborate; oxalyl dichloride; tetrabutyl ammonium fluoride; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1039/cc9960000737
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 92 percent / NaH / tetrahydrofuran / 20 h
2: 89 percent / DIBAL-H / benzene / 0.33 h / -70 °C
3: 94 percent / Ph3P, DEAD / tetrahydrofuran
4: 96 percent / TBAF / tetrahydrofuran / 1 h
5: 96 percent / NaBH4, Cu(acac)2 / ethanol / 1.5 h
With
copper acetylacetonate; sodium tetrahydroborate; tetrabutyl ammonium fluoride; sodium hydride; diisobutylaluminium hydride; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; ethanol; benzene;
DOI:10.1039/cc9960000737
