3-[5-methyl-3-[2-(methylsulfonyl)phenylsulfonyloxy]phenoxy]propoxyamine

Base Information

Chemical Name:3-[5-methyl-3-[2-(methylsulfonyl)phenylsulfonyloxy]phenoxy]propoxyamine
CAS No.:208642-91-5
Molecular Formula:C₁₇H₂₁NO₇S₂
Molecular Weight:415.488
Hs Code.:

Synonyms:3-[5-methyl-3-[2-(methylsulfonyl)phenylsulfonyloxy]phenoxy]propoxyamine

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Chemical Property of 3-[5-methyl-3-[2-(methylsulfonyl)phenylsulfonyloxy]phenoxy]propoxyamine

Chemical Property:

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Technology Process of 3-[5-methyl-3-[2-(methylsulfonyl)phenylsulfonyloxy]phenoxy]propoxyamine

There total 3 articles about 3-[5-methyl-3-[2-(methylsulfonyl)phenylsulfonyloxy]phenoxy]propoxyamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 197960-66-0
3-hydroxy-5-methylphenyl 2-(methylsulfonyl)benzenesulfonate

: 208642-91-5
3-[5-methyl-3-[2-(methylsulfonyl)phenylsulfonyloxy]phenoxy]propoxyamine

Guidance literature:: Multi-step reaction with 3 steps

1: TBP; ADDP / tetrahydrofuran

2: TPP; DEAD / tetrahydrofuran

3: 40 percent aq. NH₂CH₃ / ethanol

With bithionol; thiamine diphosphate; methylamine; 1,1'-azodicarbonyl-dipiperidine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; 1: Mitsunobu reaction / 2: Mitsunobu reaction;
DOI:10.1016/S0960-894X(03)00125-2

Reference yield:

: 208642-90-4
N-[3-[5-methyl-3-[2-(methylsulfonyl)phenylsulfonyloxy]phenoxy]propoxy]phthalimide

: 208642-91-5
3-[5-methyl-3-[2-(methylsulfonyl)phenylsulfonyloxy]phenoxy]propoxyamine

Guidance literature:: With methylamine; In ethanol;
DOI:10.1016/S0960-894X(03)00125-2

Reference yield:

: 197960-67-1
3-[5-methyl-3-[2-(methylsulfonyl)phenylsulfonyloxy]phenoxy]propanol

: 208642-91-5
3-[5-methyl-3-[2-(methylsulfonyl)phenylsulfonyloxy]phenoxy]propoxyamine

Guidance literature:: Multi-step reaction with 2 steps

1: TPP; DEAD / tetrahydrofuran

2: 40 percent aq. NH₂CH₃ / ethanol

With thiamine diphosphate; methylamine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; 1: Mitsunobu reaction;
DOI:10.1016/S0960-894X(03)00125-2