(Z)-4-methoxy-N-(6-methyl-2H-isoxazolo[2,3-b][1,2,4]thiadiazol-2-ylidene)aniline

Base Information

• Chemical Name: (Z)-4-methoxy-N-(6-methyl-2H-isoxazolo[2,3-b][1,2,4]thiadiazol-2-ylidene)aniline
• CAS No.: 1394895-37-4
• Molecular Formula: C₁₂H₁₁N₃O₂S
• Molecular Weight: 261.304

Synonyms:(Z)-4-methoxy-N-(6-methyl-2H-isoxazolo[2,3-b][1,2,4]thiadiazol-2-ylidene)aniline

Chemical Property of (Z)-4-methoxy-N-(6-methyl-2H-isoxazolo[2,3-b][1,2,4]thiadiazol-2-ylidene)aniline

Chemical Property:

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Technology Process of (Z)-4-methoxy-N-(6-methyl-2H-isoxazolo[2,3-b][1,2,4]thiadiazol-2-ylidene)aniline

There total 2 articles about (Z)-4-methoxy-N-(6-methyl-2H-isoxazolo[2,3-b][1,2,4]thiadiazol-2-ylidene)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

C12H13N3O2S (638164-94-0) → (Z)-4-methoxy-N-(6-methyl-2H-isoxazolo[2,3-b][1,2,4]thiadiazol-2-ylidene)aniline (1394895-37-4)

Guidance literature:

With iodine; In ethanol; at 20 ℃;

DOI:10.1080/17415993.2012.703671

Reference yield:

4-Methoxyphenyl isothiocyanate (2284-20-0) → (Z)-4-methoxy-N-(6-methyl-2H-isoxazolo[2,3-b][1,2,4]thiadiazol-2-ylidene)aniline (1394895-37-4)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 4 h / Reflux

2: iodine / ethanol / 20 °C

With iodine; potassium carbonate; In ethanol; acetonitrile;

DOI:10.1080/17415993.2012.703671

Reference yield: 76.0%

(Z)-4-methoxy-N-(6-methyl-2H-isoxazolo[2,3-b][1,2,4]thiadiazol-2-ylidene)aniline (1394895-37-4) + mercaptoacetic acid (68-11-1) → 3'-(4-methoxyphenyl)-6-methylspiro[isoxazolo[2,3-b][1,2,4]thiadiazole-2,2'-thiazolidin]-4'-one (1394895-46-5)

Guidance literature:

In ethanol; for 6h; Reflux;

DOI:10.1080/17415993.2012.703671

upstream raw materials:

4-Methoxyphenyl isothiocyanate

C₁₂H₁₃N₃O₂S

Downstream raw materials:

3'-(4-methoxyphenyl)-6-methylspiro[isoxazolo[2,3-b][1,2,4]thiadiazole-2,2'-thiazolidin]-4'-one

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