2,2-dimethyl-4,4-diphenyl-6-amino-1,3-dioxa-1,2,3,4-tetrahydrophenanthrene

Base Information

Chemical Name:2,2-dimethyl-4,4-diphenyl-6-amino-1,3-dioxa-1,2,3,4-tetrahydrophenanthrene
CAS No.:136197-45-0
Molecular Formula:C₂₆H₂₃NO₂
Molecular Weight:381.474
Hs Code.:

Synonyms:2,2-dimethyl-4,4-diphenyl-6-amino-1,3-dioxa-1,2,3,4-tetrahydrophenanthrene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-dimethyl-4,4-diphenyl-6-amino-1,3-dioxa-1,2,3,4-tetrahydrophenanthrene

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Technology Process of 2,2-dimethyl-4,4-diphenyl-6-amino-1,3-dioxa-1,2,3,4-tetrahydrophenanthrene

There total 3 articles about 2,2-dimethyl-4,4-diphenyl-6-amino-1,3-dioxa-1,2,3,4-tetrahydrophenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 136197-43-8
2,2-dimethyl-4,4-diphenyl-6-nitro-1,3-dioxa-1,2,3,4-tetrahydrophenanthrene

: 136197-45-0
2,2-dimethyl-4,4-diphenyl-6-amino-1,3-dioxa-1,2,3,4-tetrahydrophenanthrene

Guidance literature:: With zinc; In acetic acid; for 0.25h;

Reference yield:

: 51431-87-9
2-(diphenylmethylene)-1(2H)-naphthalenone

: 136197-45-0
2,2-dimethyl-4,4-diphenyl-6-amino-1,3-dioxa-1,2,3,4-tetrahydrophenanthrene

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / HCl / 0.33 h / 20 °C

2: 64 percent / nitric acid / acetic anhydride / 0.67 h

3: 52 percent / zinc / acetic acid / 0.25 h

With hydrogenchloride; nitric acid; zinc; In acetic anhydride; acetic acid;

Reference yield:

: 136197-37-0
2,2-dimethyl-4,4-diphenyl-1,3-dioxa-1,2,3,4-tetrahydrophenanthrene

: 136197-45-0
2,2-dimethyl-4,4-diphenyl-6-amino-1,3-dioxa-1,2,3,4-tetrahydrophenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / nitric acid / acetic anhydride / 0.67 h

2: 52 percent / zinc / acetic acid / 0.25 h

With nitric acid; zinc; In acetic anhydride; acetic acid;