1,2,5,6-tetra-O-benzyl-myo-inositol 3-(benzyl methylphosphonate) 4-(dibenzylphosphate)

Base Information

Chemical Name:1,2,5,6-tetra-O-benzyl-myo-inositol 3-(benzyl methylphosphonate) 4-(dibenzylphosphate)
CAS No.:136282-36-5
Molecular Formula:C₅₆H₅₈O₁₁P₂
Molecular Weight:969.017
Hs Code.:

Synonyms:1,2,5,6-tetra-O-benzyl-myo-inositol 3-(benzyl methylphosphonate) 4-(dibenzylphosphate)

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Chemical Property of 1,2,5,6-tetra-O-benzyl-myo-inositol 3-(benzyl methylphosphonate) 4-(dibenzylphosphate)

Chemical Property:

Purity/Quality:

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Technology Process of 1,2,5,6-tetra-O-benzyl-myo-inositol 3-(benzyl methylphosphonate) 4-(dibenzylphosphate)

There total 6 articles about 1,2,5,6-tetra-O-benzyl-myo-inositol 3-(benzyl methylphosphonate) 4-(dibenzylphosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Methyl-phosphonic acid benzyl ester (1R,2R,3R,4R,5S,6R)-2,3,4,5-tetrakis-benzyloxy-6-(bis-benzyloxy-phosphanyloxy)-cyclohexyl ester

: 136282-36-5
1,2,5,6-tetra-O-benzyl-myo-inositol 3-(benzyl methylphosphonate) 4-(dibenzylphosphate)

Guidance literature:: With tert.-butylhydroperoxide; In dichloromethane; acetonitrile; at 0 ℃; for 0.75h; Yield given;
DOI:10.1016/S0040-4020(01)86476-0

Reference yield:

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 136282-36-5
1,2,5,6-tetra-O-benzyl-myo-inositol 3-(benzyl methylphosphonate) 4-(dibenzylphosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-tetrazole / CH₂Cl₂; acetonitrile / 0.25 h

2: tert-butyl hydroperoxide / acetonitrile; CH₂Cl₂ / 0.75 h / 0 °C

With 1H-tetrazole; tert.-butylhydroperoxide; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)86476-0

Reference yield:

: 39698-23-2,64681-26-1,111466-12-7,111466-13-8,136375-67-2
1,2,5,6-tetra-O-benzyl-4-O-trans-prop-1-enyl-myo-inositol

: 136282-36-5
1,2,5,6-tetra-O-benzyl-myo-inositol 3-(benzyl methylphosphonate) 4-(dibenzylphosphate)

Guidance literature:: Multi-step reaction with 4 steps

1: 2.) N-methylimidazole / 1.) dioxane, 20 deg C, 5 min 2.) 20 deg C, 1 h

2: 0.2 N HCl / methanol; CH₂Cl₂ / 1 h / 20 °C

3: 1H-tetrazole / CH₂Cl₂; acetonitrile / 0.25 h

4: tert-butyl hydroperoxide / acetonitrile; CH₂Cl₂ / 0.75 h / 0 °C

With 1-methyl-1H-imidazole; 1H-tetrazole; hydrogenchloride; tert.-butylhydroperoxide; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)86476-0