N-(1-Benzenesulfonyl-3-methyl-2,3-dihydro-1H-indol-3-ylmethyl)-N-(2-methyl-allyl)-benzenesulfonamide

Base Information

Chemical Name:N-(1-Benzenesulfonyl-3-methyl-2,3-dihydro-1H-indol-3-ylmethyl)-N-(2-methyl-allyl)-benzenesulfonamide
CAS No.:128316-33-6
Molecular Formula:C₂₆H₂₈N₂O₄S₂
Molecular Weight:496.651
Hs Code.:

Synonyms:N-(1-Benzenesulfonyl-3-methyl-2,3-dihydro-1H-indol-3-ylmethyl)-N-(2-methyl-allyl)-benzenesulfonamide

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Chemical Property of N-(1-Benzenesulfonyl-3-methyl-2,3-dihydro-1H-indol-3-ylmethyl)-N-(2-methyl-allyl)-benzenesulfonamide

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Technology Process of N-(1-Benzenesulfonyl-3-methyl-2,3-dihydro-1H-indol-3-ylmethyl)-N-(2-methyl-allyl)-benzenesulfonamide

There total 3 articles about N-(1-Benzenesulfonyl-3-methyl-2,3-dihydro-1H-indol-3-ylmethyl)-N-(2-methyl-allyl)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 128316-31-4
2-(2'-Iodo-N-phenylsulphonylanilinyl)-4-azaphenylsulphonyl-6-methylhepta-1,6-diene

: 128316-33-6
N-(1-Benzenesulfonyl-3-methyl-2,3-dihydro-1H-indol-3-ylmethyl)-N-(2-methyl-allyl)-benzenesulfonamide

: 128316-32-5
C₂₆H₂₈N₂O₄S₂

Guidance literature:: With Ti₂CO₃; sodium formate; triphenylphosphine; palladium diacetate; In N,N-dimethyl-formamide; at 80 ℃; for 48h; Yield given;
DOI:10.1016/S0040-4020(01)88268-5

Reference yield:

: 54189-90-1
N-(2-iodophenyl)benzenesulfonamide

: 128316-33-6
N-(1-Benzenesulfonyl-3-methyl-2,3-dihydro-1H-indol-3-ylmethyl)-N-(2-methyl-allyl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1) NaH / 1) DMF, 1 h, 2) DMF, overnight, r.t.

2: 1) NaH / 1) DMF, 1 h, 2) DMF, 14 h

3: PPh₃, Tl₂CO₃, sodium formate / Pd(OAc)2 / dimethylformamide / 48 h / 80 °C

With Ti₂CO₃; sodium formate; sodium hydride; triphenylphosphine; palladium diacetate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)88268-5

Reference yield:

: 144863-34-3
3-(2'-iodo-N-phenylsulphonylanilinyl)-2-chloromethylpropene

: 128316-33-6
N-(1-Benzenesulfonyl-3-methyl-2,3-dihydro-1H-indol-3-ylmethyl)-N-(2-methyl-allyl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH / 1) DMF, 1 h, 2) DMF, 14 h

2: PPh₃, Tl₂CO₃, sodium formate / Pd(OAc)2 / dimethylformamide / 48 h / 80 °C

With Ti₂CO₃; sodium formate; sodium hydride; triphenylphosphine; palladium diacetate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)88268-5