2,2',4,4',6,6'-hexanitro(D₆)stilbene

Base Information

Chemical Name:2,2',4,4',6,6'-hexanitro(D₆)stilbene
CAS No.:120425-17-4
Molecular Formula:C₁₄H₆N₆O₁₂
Molecular Weight:456.187
Hs Code.:

2,2',4,4',6,6'-hexanitro(D<sub>6</sub>)stilbene

Synonyms:2,2',4,4',6,6'-hexanitro(D₆)stilbene

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Chemical Property of 2,2',4,4',6,6'-hexanitro(D₆)stilbene

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Technology Process of 2,2',4,4',6,6'-hexanitro(D₆)stilbene

There total 3 articles about 2,2',4,4',6,6'-hexanitro(D₆)stilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 120425-16-3
2,2',4,4',6,6'-hexanitro(D₈)bibenzyl

: 120425-17-4
2,2',4,4',6,6'-hexanitro(D₆)stilbene

Guidance literature:: With deuteriated sodium hydroxide; copper(II) sulfate; In pyridine; d⁽⁴⁾-methanol; N,N-dimethyl-formamide; at 70 ℃; for 4.5h;

Reference yield:

: 120425-15-2
[²H₅]-4,4,6-trinitrotoluene

: 120425-17-4
2,2',4,4',6,6'-hexanitro(D₆)stilbene

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / sodium deuteroxide, sodium hypochlorite / tetradeuteriomethanol; tetrahydrofuran; D₂O / 2.5 h / Ambient temperature

2: 72 percent / sodium deuteroxide, copper(II) sulfate / tetradeuteriomethanol; pyridine; dimethylformamide / 4.5 h / 70 °C

With sodium hypochlorite; deuteriated sodium hydroxide; copper(II) sulfate; In tetrahydrofuran; pyridine; d⁽⁴⁾-methanol; water-d2; N,N-dimethyl-formamide;

Reference yield:

: 120425-18-5,93951-90-7
dinitro(D₆)toluene

: 120425-17-4
2,2',4,4',6,6'-hexanitro(D₆)stilbene

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / (D₈)toluene, sulfuric acid, nitric acid

2: 57 percent / sodium deuteroxide, sodium hypochlorite / tetradeuteriomethanol; tetrahydrofuran; D₂O / 2.5 h / Ambient temperature

3: 72 percent / sodium deuteroxide, copper(II) sulfate / tetradeuteriomethanol; pyridine; dimethylformamide / 4.5 h / 70 °C

With sodium hypochlorite; deuteriated sodium hydroxide; ⁽²⁾H₈-toluene; sulfuric acid; nitric acid; copper(II) sulfate; In tetrahydrofuran; pyridine; d⁽⁴⁾-methanol; water-d2; N,N-dimethyl-formamide;