(3β,8β)-8-Acetoxymethyl-1-benzoyl-2,3-dihydro-9,10-didehydro-6-methylergoline

Base Information

Chemical Name:(3β,8β)-8-Acetoxymethyl-1-benzoyl-2,3-dihydro-9,10-didehydro-6-methylergoline
CAS No.:98260-56-1
Molecular Formula:C₂₅H₂₆N₂O₃
Molecular Weight:402.493
Hs Code.:

Synonyms:(3β,8β)-8-Acetoxymethyl-1-benzoyl-2,3-dihydro-9,10-didehydro-6-methylergoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3β,8β)-8-Acetoxymethyl-1-benzoyl-2,3-dihydro-9,10-didehydro-6-methylergoline

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Technology Process of (3β,8β)-8-Acetoxymethyl-1-benzoyl-2,3-dihydro-9,10-didehydro-6-methylergoline

There total 5 articles about (3β,8β)-8-Acetoxymethyl-1-benzoyl-2,3-dihydro-9,10-didehydro-6-methylergoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 98260-55-0
(3β,8β,9β)-8-Acetoxymethyl-1-benzoyl-9-chloro-2,3-dihydro-6-methylergoline

: 98260-56-1
(3β,8β)-8-Acetoxymethyl-1-benzoyl-2,3-dihydro-9,10-didehydro-6-methylergoline

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene; for 2h; Heating;

Reference yield:

: 98260-53-8
(3β,8β,9α)-1-Benzoyl-2,2a-dihydro-8-hydroxymethyl-6-methylergolin-9-ol

: 98260-56-1
(3β,8β)-8-Acetoxymethyl-1-benzoyl-2,3-dihydro-9,10-didehydro-6-methylergoline

Guidance literature:: Multi-step reaction with 3 steps

2: 74 percent / thionyl chloride / benzene / 1 h / 50 °C

3: DBU / benzene / 2 h / Heating

With thionyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene;

Reference yield:

: 98260-54-9
(3β,8β,9α)-8-Acetoxymethyl-1-benzoyl-2,3-dihydro-6-methylergolin-9-ol

: 98260-56-1
(3β,8β)-8-Acetoxymethyl-1-benzoyl-2,3-dihydro-9,10-didehydro-6-methylergoline

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / thionyl chloride / benzene / 1 h / 50 °C

2: DBU / benzene / 2 h / Heating

With thionyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene;