(Z)-[1-methyl-3-({[(2Z)-3-phenylprop-2-en-1-yl]oxy}methyl)-1,3-dihydro-2H-imidazol-2-ylidene]-N-oxomethanaminium chloride

Base Information

Chemical Name:(Z)-[1-methyl-3-({[(2Z)-3-phenylprop-2-en-1-yl]oxy}methyl)-1,3-dihydro-2H-imidazol-2-ylidene]-N-oxomethanaminium chloride
CAS No.:117983-39-8
Molecular Formula:C15H18 N3 O2 . Cl
Molecular Weight:307.78
Hs Code.:

Synonyms:1H-Imidazolium,2-[(hydroxyimino)methyl]-1-methyl-3-[[(3-phenyl-2-propenyl)oxy]methyl]-,chloride (9CI)

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Chemical Property of (Z)-[1-methyl-3-({[(2Z)-3-phenylprop-2-en-1-yl]oxy}methyl)-1,3-dihydro-2H-imidazol-2-ylidene]-N-oxomethanaminium chloride

Chemical Property:

Vapor Pressure:1.95E-06mmHg at 25°C
Boiling Point:394.6°Cat760mmHg
Flash Point:192.5°C
Density:g/cm³

Purity/Quality:

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Technology Process of (Z)-[1-methyl-3-({[(2Z)-3-phenylprop-2-en-1-yl]oxy}methyl)-1,3-dihydro-2H-imidazol-2-ylidene]-N-oxomethanaminium chloride

There total 3 articles about (Z)-[1-methyl-3-({[(2Z)-3-phenylprop-2-en-1-yl]oxy}methyl)-1,3-dihydro-2H-imidazol-2-ylidene]-N-oxomethanaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 117983-70-7
chloromethyl 3-phenylprop-2(E)-en-1-yl ether

: 20062-62-8
2-<(hydroxyimino)methyl>-1-methylimidazole

: 117983-39-8
2-<(hydroxyimino)methyl>-3-methyl-1-<<(3'-phenyl-2'(E)-propen-1'-yl)oxy>methyl>imidazolium chloride

Guidance literature:: In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00122a035

Reference yield:

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 117983-39-8
2-<(hydroxyimino)methyl>-3-methyl-1-<<(3'-phenyl-2'(E)-propen-1'-yl)oxy>methyl>imidazolium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 1) NaH / 1) THF, 2) room temperature, 1 h

2: 50 percent / BCl₃ / pentane; hexane / 1 h / Ambient temperature

3: 45 percent / tetrahydrofuran; dimethylformamide

With boron trichloride; sodium hydride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; pentane;
DOI:10.1021/jm00122a035

Reference yield:

: 91970-13-7
1-((E)-3-(methoxymethoxy)prop-1-enyl)benzene

: 117983-39-8
2-<(hydroxyimino)methyl>-3-methyl-1-<<(3'-phenyl-2'(E)-propen-1'-yl)oxy>methyl>imidazolium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / BCl₃ / pentane; hexane / 1 h / Ambient temperature

2: 45 percent / tetrahydrofuran; dimethylformamide

With boron trichloride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; pentane;
DOI:10.1021/jm00122a035