diethyldithiophosphatobis(4-methylphenyl isocyanide)rhodium(I)

Base Information

Chemical Name:diethyldithiophosphatobis(4-methylphenyl isocyanide)rhodium(I)
CAS No.:85253-24-3
Molecular Formula:C₂₀H₂₄N₂O₂PRhS₂
Molecular Weight:522.434
Hs Code.:

Synonyms:diethyldithiophosphatobis(4-methylphenyl isocyanide)rhodium(I)

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Chemical Property of diethyldithiophosphatobis(4-methylphenyl isocyanide)rhodium(I)

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Technology Process of diethyldithiophosphatobis(4-methylphenyl isocyanide)rhodium(I)

There total 1 articles about diethyldithiophosphatobis(4-methylphenyl isocyanide)rhodium(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 85253-22-1
{(η-cycloocta-1,5-diene)-rhodium(I)-(S2P(OC2H5)2)}

: 7175-47-5
4-methylphenyl isocyanide

: 85253-24-3
diethyldithiophosphatobis(4-methylphenyl isocyanide)rhodium(I)

Guidance literature:: In petroleum ether; under N2, petroleum ether soln. of Rh complex added dropwise to isocyanide in petroleum ether with stirring, stirred for further 5 h; ppt. filtered, dried in vac.; elem. anal.;
DOI:10.1016/S0020-1693(00)83568-9

Reference yield: 75.0%

: 85253-24-3
diethyldithiophosphatobis(4-methylphenyl isocyanide)rhodium(I)

: 670-54-2
ethenetetracarbonitrile

: diethyldithiophosphatobis(4-methylphenylisocyanide)(tetracyanoethylene)rhodium(I)-dichloromethane (1/1)

Guidance literature:: With methylene chloride; In dichloromethane; under N2, to CH2Cl2 soln. of Rh complex added TCNE, stirred for 2 h; petroleum ether added, crystals filtered, dried in vac.; elem. anal.;
DOI:10.1016/S0020-1693(00)83568-9

Reference yield: 54.0%

: 85253-24-3
diethyldithiophosphatobis(4-methylphenyl isocyanide)rhodium(I)

: 1518-16-7,6144-37-2
7,7',8,8'-tetracyanoquinodimethane

: diethyldithiophosphatobis(4-methylphenyl isocyanide)(7,7,8,8-tetracyanoquinodimethane)rhodium

Guidance literature:: In tetrahydrofuran; under N2, in hot THF; petroleum ether added, ppt. filtered, dried in vac.; elem. anal.;
DOI:10.1016/S0020-1693(00)83568-9