C₂₂H₁₇F₄NO₃

Base Information

Chemical Name:C₂₂H₁₇F₄NO₃
CAS No.:1427406-28-7
Molecular Formula:C₂₂H₁₇F₄NO₃
Molecular Weight:419.375
Hs Code.:

C<sub>22</sub>H<sub>17</sub>F<sub>4</sub>NO<sub>3</sub>

Synonyms:C₂₂H₁₇F₄NO₃

Suppliers and Price of C₂₂H₁₇F₄NO₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₂H₁₇F₄NO₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₂H₁₇F₄NO₃

There total 14 articles about C₂₂H₁₇F₄NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1427407-77-9
C₂₅H₂₃F₄NO₃

: 1427406-28-7
C₂₂H₁₇F₄NO₃

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 1214382-15-6
C₁₃H₇ClF₂O

: 1427406-28-7
C₂₂H₁₇F₄NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 2 h / 0 - 20 °C

2.1: borane-THF / tetrahydrofuran / 2 h / 60 °C / Inert atmosphere

3.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

3.2: 1 h / 20 °C

4.1: lithium hydroxide; water / tetrahydrofuran / 20 °C

With borane-THF; water; caesium carbonate; lithium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 1427407-71-3
2-(2,4-difluoro-5-methyl-phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1427406-28-7
C₂₂H₁₇F₄NO₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: dihydrogen peroxide; water; sodium hydroxide / tetrahydrofuran / 4 h / 20 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -60 °C / Inert atmosphere

3.2: 1 h / -60 - 20 °C

4.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 0 - 20 °C

4.2: 0 - 70 °C

5.1: potassium hydroxide; water / 1,4-dioxane / Reflux

6.1: tetrahydrofuran / 2 h / 0 - 20 °C

7.1: borane-THF / tetrahydrofuran / 2 h / 60 °C / Inert atmosphere

8.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

8.2: 1 h / 20 °C

9.1: lithium hydroxide; water / tetrahydrofuran / 20 °C

With 1H-imidazole; n-butyllithium; borane-THF; oxalyl dichloride; water; dihydrogen peroxide; caesium carbonate; N,N-dimethyl-formamide; potassium hydroxide; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; N,N-dimethyl-formamide;