N₁-(tert-butoxycarbonyl)-N₁₅,7-dimethyl-6-oxo-7-azaza-1,15-pentadecanediamine

Base Information

Chemical Name:N₁-(tert-butoxycarbonyl)-N₁₅,7-dimethyl-6-oxo-7-azaza-1,15-pentadecanediamine
CAS No.:214750-83-1
Molecular Formula:C₂₁H₄₃N₃O₃
Molecular Weight:385.591
Hs Code.:

N<sub>1</sub>-(tert-butoxycarbonyl)-N<sub>15</sub>,7-dimethyl-6-oxo-7-azaza-1,15-pentadecanediamine

Synonyms:N₁-(tert-butoxycarbonyl)-N₁₅,7-dimethyl-6-oxo-7-azaza-1,15-pentadecanediamine

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Chemical Property of N₁-(tert-butoxycarbonyl)-N₁₅,7-dimethyl-6-oxo-7-azaza-1,15-pentadecanediamine

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Technology Process of N₁-(tert-butoxycarbonyl)-N₁₅,7-dimethyl-6-oxo-7-azaza-1,15-pentadecanediamine

There total 1 articles about N₁-(tert-butoxycarbonyl)-N₁₅,7-dimethyl-6-oxo-7-azaza-1,15-pentadecanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6404-29-1
6-(tert-butoxycarbonylamino)hexanoic acid

: 214750-83-1
N₁-(tert-butoxycarbonyl)-N₁₅,7-dimethyl-6-oxo-7-azaza-1,15-pentadecanediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) ethyl chlorocarbomate, Et₃N / 1.) dioxane, 30 min, 2.) dioxane, RT, overnight

2: 75 percent / H₂ / 10 percent Pd/C / methanol / 0.75 h / 775.72 Torr / Ambient temperature

With hydrogen; chloroformic acid ethyl ester; triethylamine; palladium on activated charcoal; In methanol;
DOI:10.1021/jm981038d

Reference yield:

: 214750-83-1
N₁-(tert-butoxycarbonyl)-N₁₅,7-dimethyl-6-oxo-7-azaza-1,15-pentadecanediamine

: 214750-88-6
N1-<<(5,11-dihydro-6-oxo-6H-pyrido<2,3-b><1,4>benzodiazepin-11-yl)carbonyl>ethyl>-N22-<(benzyloxy)carbonyl>-7,16-dimethyl-6,17-dioxo-7,16-diaza-1,22-docosanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) ethyl chlorocarbomate, Et₃N / 1.) dioxane, 30 min, 2.) dioxane, RT, overnight

2: 96 percent / 6N aq. HCl / tetrahydrofuran / 2 h / Ambient temperature

3: 43 percent / Et₃N, KI / CH₂Cl₂

With hydrogenchloride; chloroformic acid ethyl ester; triethylamine; potassium iodide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm981038d

Reference yield:

: 214750-83-1
N₁-(tert-butoxycarbonyl)-N₁₅,7-dimethyl-6-oxo-7-azaza-1,15-pentadecanediamine

: 214750-87-5
N1,N1-bis<<(5,11-dihydro-6-oxo-6H-pyrido<2,3-b><1,4>benzodiazepin-11-yl)carbonyl>methyl>-N22-<(benzyloxy)carbonyl>-7,16-dimethyl-6,17-dioxo-7,16-diaza-1,22-docosanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) ethyl chlorocarbomate, Et₃N / 1.) dioxane, 30 min, 2.) dioxane, RT, overnight

2: 96 percent / 6N aq. HCl / tetrahydrofuran / 2 h / Ambient temperature

3: 27 percent / Et₃N, KI / CH₂Cl₂

With hydrogenchloride; chloroformic acid ethyl ester; triethylamine; potassium iodide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm981038d