2-ethyl-3-methyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)butanamide

Base Information

Chemical Name:2-ethyl-3-methyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)butanamide
CAS No.:1407870-28-3
Molecular Formula:C₁₄H₁₄F₇NO
Molecular Weight:345.26
Hs Code.:

Synonyms:2-ethyl-3-methyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)butanamide

Suppliers and Price of 2-ethyl-3-methyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)butanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-ethyl-3-methyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)butanamide

Chemical Property:

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Technology Process of 2-ethyl-3-methyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)butanamide

There total 2 articles about 2-ethyl-3-methyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56006-49-6,32444-32-9
2-ethyl-3-methyl-butyric acid

: 1407870-28-3
2-ethyl-3-methyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)butanamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane / 0 - 20 °C / Inert atmosphere

2: toluene / 16 h / 20 °C / Reflux

With oxalyl dichloride; In dichloromethane; toluene;
DOI:10.1021/ja309325e

Reference yield:

: 51760-89-5
2-ethyl-3-methyl-butyryl chloride

: 651-83-2
4-trifluoromethyl-2,3,5,6-tetrafluoroaniline

: 1407870-28-3
2-ethyl-3-methyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)butanamide

Guidance literature:: In toluene; at 20 ℃; for 16h; Reflux;
DOI:10.1021/ja309325e

Reference yield: 82.0%

: 624-31-7
4-tolyl iodide

: 1407870-28-3
2-ethyl-3-methyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)butanamide

: 2-isopropyl-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-3-p-tolylbutanamide

Guidance literature:: With potassium dihydrogenphosphate; palladium(II) trifluoroacetate; 2-isobutoxyquinoline; silver carbonate; In hexane; at 110 ℃; for 24h; Sealed tube;
DOI:10.1021/ja309325e