C₃H₃BS(C₆H₅)(C₄H₉)(C₆F₅)2

Base Information

• Chemical Name: C₃H₃BS(C₆H₅)(C₄H₉)(C₆F₅)2
• CAS No.: 1311031-11-4
• Molecular Formula: C₂₅H₁₇BF₁₀S
• Molecular Weight: 550.271
• Mol file: 1311031-11-4.mol

Synonyms:C₃H₃BS(C₆H₅)(C₄H₉)(C₆F₅)2

Chemical Property of C₃H₃BS(C₆H₅)(C₄H₉)(C₆F₅)2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃H₃BS(C₆H₅)(C₄H₉)(C₆F₅)2

There total 4 articles about C₃H₃BS(C₆H₅)(C₄H₉)(C₆F₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

(C6H5)SCH2B(C6F5)2 (1311031-15-8) + hex-1-yne (693-02-7) → C3H3BS(C6H5)(C4H9)(C6F5)2 (1311031-11-4)

Guidance literature:

In toluene; (N2); using Schlenk techniques; dissolving of PhSCH2B(C6F5)2 in toluene at -38°C, addn. of HCCC4H9 via syringe, stirring overnight; evapn. of solvent, addn. of cold pentane, freezing overnight, pptn.; elem. anal.;

DOI:10.1021/om200336t

Reference yield:

bis(pentafluorophenyl)boron chloride (2720-03-8) → C3H3BS(C6H5)(C4H9)(C6F5)2 (1311031-11-4)

Guidance literature:

Multi-step reaction with 2 steps

1: n-BuLi / diethyl ether; hexane

2: toluene

With n-BuLi; In diethyl ether; hexane; toluene;

DOI:10.1021/om200336t

Reference yield:

methyl-phenyl-thioether (100-68-5) → C3H3BS(C6H5)(C4H9)(C6F5)2 (1311031-11-4)

Guidance literature:

Multi-step reaction with 2 steps

1: n-BuLi / diethyl ether; hexane

2: toluene

With n-BuLi; In diethyl ether; hexane; toluene;

DOI:10.1021/om200336t

upstream raw materials:

(C₆H₅)SCH₂B(C₆F₅)2

hex-1-yne

methyl-phenyl-thioether

2-bromo-1-(methylsulfanyl)benzene