N-benzyl-2-[1-(1,3-dimethylindol-2-yl)ethylidene]-3-isopropylidenesuccinimide

Base Information

Chemical Name:N-benzyl-2-[1-(1,3-dimethylindol-2-yl)ethylidene]-3-isopropylidenesuccinimide
CAS No.:253325-58-5
Molecular Formula:C₂₆H₂₆N₂O₂
Molecular Weight:398.505
Hs Code.:

Synonyms:N-benzyl-2-[1-(1,3-dimethylindol-2-yl)ethylidene]-3-isopropylidenesuccinimide

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Chemical Property of N-benzyl-2-[1-(1,3-dimethylindol-2-yl)ethylidene]-3-isopropylidenesuccinimide

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Technology Process of N-benzyl-2-[1-(1,3-dimethylindol-2-yl)ethylidene]-3-isopropylidenesuccinimide

There total 7 articles about N-benzyl-2-[1-(1,3-dimethylindol-2-yl)ethylidene]-3-isopropylidenesuccinimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 144498-74-8
(E)-3-[1-(1,3-dimethyl-1H-indol-2-yl)ethylidene]-4-isopropylidenetetrahydrofuran-2,5-dione

: 100-46-9
benzylamine

: 253325-58-5
N-benzyl-2-[1-(1,3-dimethylindol-2-yl)ethylidene]-3-isopropylidenesuccinimide

Guidance literature:: (E)-3-[1-(1,3-dimethyl-1H-indol-2-yl)ethylidene]-4-isopropylidenetetrahydrofuran-2,5-dione; benzylamine; In benzene; at 20 ℃; for 1h;

With 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride; In benzene; at 80 ℃; for 5h;
DOI:10.1016/S0040-4039(99)01702-5

Reference yield:

: 83-34-1
3-Methylindole

: 253325-58-5
N-benzyl-2-[1-(1,3-dimethylindol-2-yl)ethylidene]-3-isopropylidenesuccinimide

Guidance literature:: Multi-step reaction with 6 steps

1.1: NaH / dimethylformamide

1.2: dimethylformamide

2.1: BF₃*Et₂O; CH₃COOH / 20 °C

3.1: NaH / toluene

3.2: HCl

4.1: KOH / ethanol

5.1: DCC

6.1: 85 percent / ZnCl₂; hexamethyldisilazane / benzene / Heating

With potassium hydroxide; boron trifluoride diethyl etherate; sodium hydride; acetic acid; dicyclohexyl-carbodiimide; 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride; In ethanol; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1039/b002374o

Reference yield:

: 875-30-9
1,3-dimethylindole

: 253325-58-5
N-benzyl-2-[1-(1,3-dimethylindol-2-yl)ethylidene]-3-isopropylidenesuccinimide

Guidance literature:: Multi-step reaction with 5 steps

1.1: BF₃*Et₂O; CH₃COOH / 20 °C

2.1: NaH / toluene

2.2: HCl

3.1: KOH / ethanol

4.1: DCC

5.1: 85 percent / ZnCl₂; hexamethyldisilazane / benzene / Heating

With potassium hydroxide; boron trifluoride diethyl etherate; sodium hydride; acetic acid; dicyclohexyl-carbodiimide; 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride; In ethanol; toluene; benzene;
DOI:10.1039/b002374o