1,3-dihydroxy-1,3-diphenylbenzindan-2-one 2-oxime

Base Information

Chemical Name:1,3-dihydroxy-1,3-diphenylbenzindan-2-one 2-oxime
CAS No.:75155-48-5
Molecular Formula:C₂₅H₁₉NO₃
Molecular Weight:381.431
Hs Code.:

1,3-dihydroxy-1,3-diphenylbenz<f>indan-2-one 2-oxime

Synonyms:1,3-dihydroxy-1,3-diphenylbenzindan-2-one 2-oxime

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Chemical Property of 1,3-dihydroxy-1,3-diphenylbenzindan-2-one 2-oxime

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Technology Process of 1,3-dihydroxy-1,3-diphenylbenzindan-2-one 2-oxime

There total 6 articles about 1,3-dihydroxy-1,3-diphenylbenzindan-2-one 2-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 75155-47-4
benzindane-1,2,3-trione 2-oxime

: phenylmagnesium bromide

: 75155-48-5
1,3-dihydroxy-1,3-diphenylbenzindan-2-one 2-oxime

Guidance literature:: In diethyl ether; benzene; for 3h; Heating;

Reference yield:

: 22734-61-8
1H-cyclopenta[b]naphthalene-1,3(2H)-dione

: 75155-48-5
1,3-dihydroxy-1,3-diphenylbenzindan-2-one 2-oxime

Guidance literature:: Multi-step reaction with 2 steps

1: HNO₂

With cis-nitrous acid;
DOI:10.1039/c39800000463

Reference yield:

: 22734-61-8
1H-cyclopenta[b]naphthalene-1,3(2H)-dione

: 75155-48-5,85970-13-4,85970-14-5
(1S,3S)-1,3-Dihydroxy-1,3-diphenyl-1,3-dihydro-cyclopenta[b]naphthalen-2-one oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / sodium hydroxide, sodium nitrite, hydrochloric acid / H₂O / 0.5 h / 0 °C

2: diethyl ether / 0.08 h / 0 °C

With hydrogenchloride; sodium hydroxide; sodium nitrite; In diethyl ether; water;