9-(3,5-di-O-benzoyl-2-deoxy-2-fluoro-β-L-arabinofuranosyl)-9H-6-chloropurine

Base Information

• Chemical Name: 9-(3,5-di-O-benzoyl-2-deoxy-2-fluoro-β-L-arabinofuranosyl)-9H-6-chloropurine
• CAS No.: 193754-02-8
• Molecular Formula: C₂₄H₁₈ClFN₄O₅
• Molecular Weight: 496.882

Synonyms:9-(3,5-di-O-benzoyl-2-deoxy-2-fluoro-β-L-arabinofuranosyl)-9H-6-chloropurine

Chemical Property of 9-(3,5-di-O-benzoyl-2-deoxy-2-fluoro-β-L-arabinofuranosyl)-9H-6-chloropurine

Chemical Property:

Purity/Quality:

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Technology Process of 9-(3,5-di-O-benzoyl-2-deoxy-2-fluoro-β-L-arabinofuranosyl)-9H-6-chloropurine

There total 1 articles about 9-(3,5-di-O-benzoyl-2-deoxy-2-fluoro-β-L-arabinofuranosyl)-9H-6-chloropurine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-chloropurine (87-42-3) + 1-bromo-2-deoxy-2-β-fluoro-3,5-di-O-benzoyl-α-L-arabinose (171866-29-8) → 9-(3,5-di-O-benzoyl-2-deoxy-2-fluoro-β-L-arabinofuranosyl)-9H-6-chloropurine (193754-02-8)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) CH₃CN, RT, 30 min, 2.) CH₃CN, RT, 4 h;

DOI:10.1021/jm970233+

Reference yield: 82.0%

9-(3,5-di-O-benzoyl-2-deoxy-2-fluoro-β-L-arabinofuranosyl)-9H-6-chloropurine (193754-02-8) → C24H19FN4O5S

Guidance literature:

With thiourea; In ethanol; for 2h; Heating;

DOI:10.1021/jm970233+

Reference yield:

9-(3,5-di-O-benzoyl-2-deoxy-2-fluoro-β-L-arabinofuranosyl)-9H-6-chloropurine (193754-02-8) → C24H19FN4O5 (193754-03-9)

Guidance literature:

With hydrogen; triethylamine; palladium on activated charcoal; In ethyl acetate; for 5h; under 2068.6 Torr;

DOI:10.1021/jm970233+

upstream raw materials:

6-chloropurine

1-bromo-2-deoxy-2-β-fluoro-3,5-di-O-benzoyl-α-L-arabinose

Downstream raw materials:

C₂₆H₂₄FN₅O₅

C₂₇H₂₄FN₅O₅

C₂₄H₁₉FN₄O₅

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