(N,N'-diisopropylaminotroponiminate)AlCy₂

Base Information

Chemical Name:(N,N'-diisopropylaminotroponiminate)AlCy₂
CAS No.:365215-42-5
Molecular Formula:C₂₅H₄₁AlN₂
Molecular Weight:396.595
Hs Code.:

(N,N'-diisopropylaminotroponiminate)AlCy<sub>2</sub>

Synonyms:(N,N'-diisopropylaminotroponiminate)AlCy₂

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Chemical Property of (N,N'-diisopropylaminotroponiminate)AlCy₂

Chemical Property:

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Technology Process of (N,N'-diisopropylaminotroponiminate)AlCy₂

There total 2 articles about (N,N'-diisopropylaminotroponiminate)AlCy₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 365215-41-4
(N,N'-diisopropylaminotroponiminate)AlCl₂

: 931-51-1
cyclohexylmagnesiumchloride

: 365215-42-5
(N,N'-diisopropylaminotroponiminate)AlCy₂

Guidance literature:: In diethyl ether; hexane; under N2 atm. soln. (iPr2-ATI)AlCl2 in hexane was cooled to -37°Cand CyMgCl in Et2O was added, soln. was stirred for 16 h; solvent was evapd. under vac., residue was dissolved in pentane, dioxanewas added, soln. was cooled to -37°C for 16 h, ppt. was filtered off, filtrate was evapd., residue was dissolved in pentane and kept at -37°C for 16 h;
DOI:10.1021/ja010242e

Reference yield:

: lithium N,N-diisopropylaminotroponiminate

: 365215-42-5
(N,N'-diisopropylaminotroponiminate)AlCy₂

Guidance literature:: Multi-step reaction with 2 steps

1: toluene

2: hexane; diethyl ether

In diethyl ether; hexane; toluene;
DOI:10.1021/ja010242e

Reference yield:

: 365215-42-5
(N,N'-diisopropylaminotroponiminate)AlCy₂

: trityl tetrakis(pentafluorophenyl)borate

: 365215-50-5
(N,N'-diisopropylaminotroponiminate)AlCy(C₆F₅)

: 1109-15-5
tris(pentafluorophenyl)borate

Guidance literature:: In pentane; byproducts: Ph3CH; under N2 atm. to soln. (iPr2-ATI)AlCy2 was added (Ph3C)(B(C6F5)4) and stirred at 25°C for 24 h; not isolated, identified by NMR;
DOI:10.1021/ja010242e