5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

Base Information

Chemical Name:5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine
CAS No.:228412-67-7
Molecular Formula:C₂₆H₂₇FN₄O₁₆
Molecular Weight:670.516
Hs Code.:

5-fluoro-N-<4-O-<methyl (2,3,4-tri-O-acetyl-β-D-glucopyranosyl)uronate>-3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

Synonyms:5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

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Chemical Property of 5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

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Technology Process of 5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

There total 3 articles about 5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 51-21-8
5-fluorouracil

: 228412-65-5
N-<4-O--3-nitrobenzyloxycarbonyl>acetoxymethylamine

: 228412-67-7
5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 18h; Ambient temperature;

Reference yield:

: 148580-01-2
(2S,3S,4S,5R,6S)-3,4,5-Triacetoxy-6-[2-nitro-4-(4-nitro-phenoxycarbonyloxymethyl)-phenoxy]-tetrahydro-pyran-2-carboxylic acid methyl ester

: 228412-67-7
5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / NEt₃ / dimethylformamide / 18 h / Ambient temperature

2: 50 percent / pyridine / toluene; tetrahydrofuran / 4 h / Heating

3: 64 percent / NEt₃ / dimethylformamide / 18 h / Ambient temperature

With pyridine; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;

Reference yield:

: 228412-63-3
N-<4-O--3-nitrobenzyloxycarbonyl>glycine

: 228412-67-7
5-fluoro-N-<4-O--3-nitrobenzyloxycarbonyl>-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-ylmethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / pyridine / toluene; tetrahydrofuran / 4 h / Heating

2: 64 percent / NEt₃ / dimethylformamide / 18 h / Ambient temperature

With pyridine; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;