(1R,3R)-3-((tert-butoxycarbonyl)amino)cyclohexanecarboxylic acid

Base Information

• Chemical Name: (1R,3R)-3-((tert-butoxycarbonyl)amino)cyclohexanecarboxylic acid
• CAS No.: 1430938-32-1
• Molecular Formula: C₁₂H₂₁NO₄
• Molecular Weight: 243.303
• Hs Code.: 2924297099

Synonyms:(1R,3R)-3-((tert-butoxycarbonyl)amino)cyclohexanecarboxylic acid

Chemical Property of (1R,3R)-3-((tert-butoxycarbonyl)amino)cyclohexanecarboxylic acid

Chemical Property:

• Boiling Point: 396.7±31.0 °C(Predicted)
• Density: 1.12±0.1 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

(1R,3R)-3-Boc-amino-cyclohexanecarboxylicacid 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of (1R,3R)-3-((tert-butoxycarbonyl)amino)cyclohexanecarboxylic acid

There total 4 articles about (1R,3R)-3-((tert-butoxycarbonyl)amino)cyclohexanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

(1R,3R)-3-(4-methoxyphenyl)cyclohexyl-tert-butylcarbamate → (1R,3R)-3-((tert-butoxycarbonyl)amino)cyclohexanecarboxylic acid (1430938-32-1,218772-92-0,222530-33-8)

Guidance literature:

With sodium periodate; ruthenium(III) trichloride hydrate; In water; ethyl acetate; acetonitrile; at 20 ℃; for 1.5h;

DOI:10.1002/adsc.201400824

Reference yield:

N-[(1R,3R)-3-(4-methoxyphenyl)cyclohexyl]-4-methylbenzenesulfonamide → (1R,3R)-3-((tert-butoxycarbonyl)amino)cyclohexanecarboxylic acid (1430938-32-1,218772-92-0,222530-33-8)

Guidance literature:

Multi-step reaction with 3 steps

1: dmap / acetonitrile / 3 h / 20 °C

2: magnesium / methanol / 1 h / 20 °C / Sonication

3: ruthenium(III) trichloride hydrate; sodium periodate / water; acetonitrile; ethyl acetate / 1.5 h / 20 °C

With dmap; sodium periodate; ruthenium(III) trichloride hydrate; magnesium; In methanol; water; ethyl acetate; acetonitrile;

DOI:10.1002/adsc.201400824

Reference yield:

C25H33NO5S → (1R,3R)-3-((tert-butoxycarbonyl)amino)cyclohexanecarboxylic acid (1430938-32-1,218772-92-0,222530-33-8)

Guidance literature:

Multi-step reaction with 2 steps

1: magnesium / methanol / 1 h / 20 °C / Sonication

2: ruthenium(III) trichloride hydrate; sodium periodate / water; acetonitrile; ethyl acetate / 1.5 h / 20 °C

With sodium periodate; ruthenium(III) trichloride hydrate; magnesium; In methanol; water; ethyl acetate; acetonitrile;

DOI:10.1002/adsc.201400824

upstream raw materials:

di-tert-butyl dicarbonate

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