(+)-pinanediol (1R)-2-[3-(tert-butoxycarbonyl)phenyl]-1-(2-thienylacetylamino)ethaneboronate

Base Information

Chemical Name:(+)-pinanediol (1R)-2-[3-(tert-butoxycarbonyl)phenyl]-1-(2-thienylacetylamino)ethaneboronate
CAS No.:1154427-25-4
Molecular Formula:C₂₉H₃₈BNO₅S
Molecular Weight:523.501
Hs Code.:

Synonyms:(+)-pinanediol (1R)-2-[3-(tert-butoxycarbonyl)phenyl]-1-(2-thienylacetylamino)ethaneboronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-pinanediol (1R)-2-[3-(tert-butoxycarbonyl)phenyl]-1-(2-thienylacetylamino)ethaneboronate

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Technology Process of (+)-pinanediol (1R)-2-[3-(tert-butoxycarbonyl)phenyl]-1-(2-thienylacetylamino)ethaneboronate

There total 1 articles about (+)-pinanediol (1R)-2-[3-(tert-butoxycarbonyl)phenyl]-1-(2-thienylacetylamino)ethaneboronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39098-97-0
2-thienylacetic acid chloride

: C₂₃H₃₄BNO₄

: 1154427-25-4
(+)-pinanediol (1R)-2-[3-(tert-butoxycarbonyl)phenyl]-1-(2-thienylacetylamino)ethaneboronate

Guidance literature:: 2-thienylacetic acid chloride; C₂₃H₃₄BNO₄; In tetrahydrofuran; hexane; at -78 - 20 ℃;

With water; In tetrahydrofuran; hexane;

Reference yield: 47.0%

: 1154427-25-4
(+)-pinanediol (1R)-2-[3-(tert-butoxycarbonyl)phenyl]-1-(2-thienylacetylamino)ethaneboronate

: 1154426-00-2
(1R)-1-(2-thiophene-2-yl-acetylamino)-2-(3-carboxyphenyl)ethyl-1-boronic acid

Guidance literature:: With hydrogenchloride; water; In 1,4-dioxane; at 100 ℃; for 0.916667h;

Reference yield:

: 1154427-25-4
(+)-pinanediol (1R)-2-[3-(tert-butoxycarbonyl)phenyl]-1-(2-thienylacetylamino)ethaneboronate

: 1429253-81-5
C₂₅H₃₀BNO₅S

Guidance literature:: With methoxybenzene; trifluoroacetic acid; In dichloromethane; at -10 - 20 ℃; for 3.16667h; Inert atmosphere;
DOI:10.1021/jm301490d