N-Benzoyl-N-{9-[3-(bis-chloromethyl-methyl-silanyl)-propyl]-9H-purin-6-yl}-benzamide

Base Information

Chemical Name:N-Benzoyl-N-{9-[3-(bis-chloromethyl-methyl-silanyl)-propyl]-9H-purin-6-yl}-benzamide
CAS No.:191086-70-1
Molecular Formula:C₂₅H₂₅Cl₂N₅O₂Si
Molecular Weight:526.497
Hs Code.:

Synonyms:N-Benzoyl-N-{9-[3-(bis-chloromethyl-methyl-silanyl)-propyl]-9H-purin-6-yl}-benzamide

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Chemical Property of N-Benzoyl-N-{9-[3-(bis-chloromethyl-methyl-silanyl)-propyl]-9H-purin-6-yl}-benzamide

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Technology Process of N-Benzoyl-N-{9-[3-(bis-chloromethyl-methyl-silanyl)-propyl]-9H-purin-6-yl}-benzamide

There total 3 articles about N-Benzoyl-N-{9-[3-(bis-chloromethyl-methyl-silanyl)-propyl]-9H-purin-6-yl}-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 2043-09-6
Methyl-bis-chlormethylsilan

: 191086-68-7
N-(9-Allyl-9H-purin-6-yl)-N-benzoyl-benzamide

: 191086-70-1
N-Benzoyl-N-{9-[3-(bis-chloromethyl-methyl-silanyl)-propyl]-9H-purin-6-yl}-benzamide

Guidance literature:: With dihydrogen hexachloroplatinate; isopropyl alcohol; In tetrahydrofuran; at 60 ℃; for 2h;
DOI:10.1021/jo962165p

Reference yield:

: 66224-66-6,66224-67-7,66224-68-8,66224-69-9,134434-48-3,134434-49-4,134454-76-5,134461-75-9
adenine

: 191086-70-1
N-Benzoyl-N-{9-[3-(bis-chloromethyl-methyl-silanyl)-propyl]-9H-purin-6-yl}-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / sodium hydride / dimethylformamide / 2 h / 70 °C

2: 50 percent / pyridine / 3 h / Ambient temperature

3: 58 percent / H₂PtCl₆, propan-2-ol / tetrahydrofuran / 2 h / 60 °C

With pyridine; dihydrogen hexachloroplatinate; sodium hydride; isopropyl alcohol; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo962165p

Reference yield:

: 4121-39-5
9-allyl-9H-adenine

: 191086-70-1
N-Benzoyl-N-{9-[3-(bis-chloromethyl-methyl-silanyl)-propyl]-9H-purin-6-yl}-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / pyridine / 3 h / Ambient temperature

2: 58 percent / H₂PtCl₆, propan-2-ol / tetrahydrofuran / 2 h / 60 °C

With pyridine; dihydrogen hexachloroplatinate; isopropyl alcohol; In tetrahydrofuran;
DOI:10.1021/jo962165p