C₁₈H₂₄INO₂S

Base Information

Chemical Name:C₁₈H₂₄INO₂S
CAS No.:1383385-92-9
Molecular Formula:C₁₈H₂₄INO₂S
Molecular Weight:445.365
Hs Code.:

C<sub>18</sub>H<sub>24</sub>INO<sub>2</sub>S

Synonyms:C₁₈H₂₄INO₂S

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Chemical Property of C₁₈H₂₄INO₂S

Chemical Property:

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Technology Process of C₁₈H₂₄INO₂S

There total 10 articles about C₁₈H₂₄INO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1383385-76-9
C₁₉H₂₆INO₂S

: 1383385-92-9
C₁₈H₂₄INO₂S

Guidance literature:: C₁₉H₂₆INO₂S; With lithium hydroxide; In tetrahydrofuran;

With phosphoric acid; In tetrahydrofuran;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1383385-92-9
C₁₈H₂₄INO₂S

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 8 h / -78 °C / Inert atmosphere

2.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide; water / 4 h / 90 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

3.2: 2 h / -78 - 20 °C

4.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water / 2 h / 80 °C / Inert atmosphere

5.1: hydrogen / palladium 10% on activated carbon / methanol / 15 h / 2585.81 Torr

6.1: acetonitrile / 3 h / 80 °C

7.1: sodium tetrahydroborate / methanol / 1 h

8.1: lithium diisopropyl amide / n-heptane; tetrahydrofuran; ethylbenzene / 2.5 h / -78 °C / Inert atmosphere

8.2: 1.5 h / -78 °C

9.1: lithium hydroxide / tetrahydrofuran

With sodium tetrahydroborate; n-butyllithium; hydrogen; sodium hexamethyldisilazane; sodium carbonate; lithium hydroxide; lithium diisopropyl amide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; In tetrahydrofuran; methanol; n-heptane; ethylbenzene; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 22288-78-4
Methyl 3-aminothiophene-2-carboxylate

: 1383385-92-9
C₁₈H₂₄INO₂S

Guidance literature:: Multi-step reaction with 7 steps

1.1: diiodomethane; tert.-butylnitrite / acetonitrile / 1.5 h / 50 °C

2.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water / 2 h / 80 °C / Inert atmosphere

3.1: hydrogen / palladium 10% on activated carbon / methanol / 15 h / 2585.81 Torr

4.1: acetonitrile / 3 h / 80 °C

5.1: sodium tetrahydroborate / methanol / 1 h

6.1: lithium diisopropyl amide / n-heptane; tetrahydrofuran; ethylbenzene / 2.5 h / -78 °C / Inert atmosphere

6.2: 1.5 h / -78 °C

7.1: lithium hydroxide / tetrahydrofuran

With sodium tetrahydroborate; tert.-butylnitrite; diiodomethane; hydrogen; sodium carbonate; lithium hydroxide; lithium diisopropyl amide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; In tetrahydrofuran; methanol; n-heptane; ethylbenzene; water; acetonitrile;