C₄₁H₇₆BrNO₃Si₃

Base Information

Chemical Name:C₄₁H₇₆BrNO₃Si₃
CAS No.:1448446-17-0
Molecular Formula:C₄₁H₇₆BrNO₃Si₃
Molecular Weight:795.22
Hs Code.:

C<sub>41</sub>H<sub>76</sub>BrNO<sub>3</sub>Si<sub>3</sub>

Synonyms:C₄₁H₇₆BrNO₃Si₃

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Chemical Property of C₄₁H₇₆BrNO₃Si₃

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Technology Process of C₄₁H₇₆BrNO₃Si₃

There total 10 articles about C₄₁H₇₆BrNO₃Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1448446-16-9
C₁₇H₂₆Br₂Si

: 1448446-08-9
C₃₀H₆₂BNO₅Si₂

: 1448446-17-0
C₄₁H₇₆BrNO₃Si₃

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; thallium (I) ethoxide; In tetrahydrofuran; water; at 20 ℃; stereoselective reaction; Inert atmosphere;

Reference yield:

: 138124-05-7
(1S,6R)-(-)-8-Oxabicyclo<4.3.0>non-2-en-7-one

: 1448446-17-0
C₄₁H₇₆BrNO₃Si₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - -30 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane / 0.42 h / -78 °C / Inert atmosphere

3.1: diisopropylamine / diethyl ether; tetrahydrofuran; hexane / 0.33 h / -78 - -50 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

5.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 20 °C

6.1: dimethyl sulfoxide; oxalyl dichloride; N-ethyl-N,N-diisopropylamine / dichloromethane / -78 - 20 °C / Inert atmosphere

7.1: triphenylphosphine; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

8.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; thallium (I) ethoxide / tetrahydrofuran; water / 20 °C / Inert atmosphere

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; oxalyl dichloride; thallium (I) ethoxide; diisobutylaluminium hydride; dimethyl sulfoxide; diisopropylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; 8.1: |Suzuki Coupling;

Reference yield:

: 4949-20-6,52192-01-5
(E)-2,4-pentadien-1-ol

: 1448446-17-0
C₄₁H₇₆BrNO₃Si₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: dimethyl zinc(II); methylmagnesium bromide; (+)-1,1'-binaphthalene-8,8'-diol / dichloromethane; toluene; diethyl ether / 0 - 20 °C / Inert atmosphere

2.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - -30 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane / 0.42 h / -78 °C / Inert atmosphere

4.1: diisopropylamine / diethyl ether; tetrahydrofuran; hexane / 0.33 h / -78 - -50 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

5.2: -78 - 20 °C / Inert atmosphere

6.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 20 °C

7.1: dimethyl sulfoxide; oxalyl dichloride; N-ethyl-N,N-diisopropylamine / dichloromethane / -78 - 20 °C / Inert atmosphere

8.1: triphenylphosphine; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

9.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; thallium (I) ethoxide / tetrahydrofuran; water / 20 °C / Inert atmosphere

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; oxalyl dichloride; methylmagnesium bromide; dimethyl zinc(II); thallium (I) ethoxide; diisobutylaluminium hydride; dimethyl sulfoxide; diisopropylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; (+)-1,1'-binaphthalene-8,8'-diol; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; toluene; 9.1: |Suzuki Coupling;