C₂₆H₂₄N₂O₅S

Base Information

Chemical Name:C₂₆H₂₄N₂O₅S
CAS No.:856906-37-1
Molecular Formula:C₂₆H₂₄N₂O₅S
Molecular Weight:476.553
Hs Code.:

C<sub>26</sub>H<sub>24</sub>N<sub>2</sub>O<sub>5</sub>S

Synonyms:C₂₆H₂₄N₂O₅S

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Chemical Property of C₂₆H₂₄N₂O₅S

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Technology Process of C₂₆H₂₄N₂O₅S

There total 12 articles about C₂₆H₂₄N₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 856906-36-0
C₂₀H₂₀N₂O₅

: 108-98-5
thiophenol

: 856906-37-1
C₂₆H₂₄N₂O₅S

Guidance literature:: C₂₀H₂₀N₂O₅; With pyridinium hydrobromide perbromide; In dichloromethane; at 23 ℃; for 17h; Inert atmosphere;

thiophenol; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 0 ℃; for 0.416667h; Inert atmosphere;

Reference yield:

: C₂₀H₁₉BrN₂O₅

: 108-98-5
thiophenol

: 856906-37-1
C₂₆H₂₄N₂O₅S

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In DMF (N,N-dimethyl-formamide); at 0 ℃; for 0.416667h;

Reference yield:

: C₃₂H₅₀N₂O₆Si₂

: 856906-37-1
C₂₆H₂₄N₂O₅S

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium trifluoromethanesulfonate / toluene / 3 h / 23 - 60 °C / Inert atmosphere

1.2: 18 h / 23 °C / Inert atmosphere

2.1: diethylazodicarboxylate; triphenylphosphine / toluene / 1.5 h / 0 °C / Inert atmosphere

2.2: 23 h / 0 - 23 °C / Inert atmosphere

3.1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 5.5 h / 0 - 23 °C / Inert atmosphere

4.1: 2-iodoxybenzoic acid / dimethyl sulfoxide / 36 h / 23 °C / Inert atmosphere

5.1: pyridinium hydrobromide perbromide / dichloromethane / 17 h / 23 °C / Inert atmosphere

5.2: 0.42 h / 0 °C / Inert atmosphere

With 2-iodoxybenzoic acid; tetrabutyl ammonium fluoride; lithium trifluoromethanesulfonate; acetic acid; pyridinium hydrobromide perbromide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene;