Technology Process of C26H27NO6
There total 7 articles about C26H27NO6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C26H23NO6;
With
methylamine;
In
tetrahydrofuran; water;
at 21 - 23 ℃;
for 26h;
benzyl chloroformate;
With
potassium carbonate;
In
tetrahydrofuran; water;
at 20 ℃;
for 28h;
With
hydrogenchloride;
In
water;
pH=~ 5;
- Guidance literature:
-
C18H21NO4; benzyl chloroformate;
With
potassium carbonate;
In
tetrahydrofuran; water;
at 0 - 20 ℃;
for 28h;
With
hydrogenchloride;
In
water;
pH=~ 5;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: pyridine / isopropyl alcohol / 8 h / 80 - 82 °C
2.1: sodium hydride / tetra-(n-butyl)ammonium iodide / tetrahydrofuran; mineral oil / 18.5 h / -15 - 20 °C
3.1: ozone / dichloromethane / -70 °C
4.1: 2-methyl-but-2-ene; sodium hypochlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol; tetrahydrofuran / 4 h / 10 - 20 °C
5.1: methylamine / water; tetrahydrofuran / 26 h / 5 - 23 °C
6.1: potassium carbonate / water; tetrahydrofuran / 28 h / 0 - 20 °C
6.2: pH ~ 5
With
sodium hypochlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium hydride; potassium carbonate; ozone; methylamine;
pyridine; tetra-(n-butyl)ammonium iodide;
In
tetrahydrofuran; dichloromethane; water; isopropyl alcohol; mineral oil; tert-butyl alcohol;
4.1: Pinnick Oxidation;
