6-(2-ethoxymorpholino)-2-(4-methoxy-3-nitrobenzylsulfanyl)-9-methyl-9H-purine

Base Information

Chemical Name:6-(2-ethoxymorpholino)-2-(4-methoxy-3-nitrobenzylsulfanyl)-9-methyl-9H-purine
CAS No.:1253848-25-7
Molecular Formula:C₂₀H₂₄N₆O₅S
Molecular Weight:460.514
Hs Code.:

Synonyms:6-(2-ethoxymorpholino)-2-(4-methoxy-3-nitrobenzylsulfanyl)-9-methyl-9H-purine

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Chemical Property of 6-(2-ethoxymorpholino)-2-(4-methoxy-3-nitrobenzylsulfanyl)-9-methyl-9H-purine

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Technology Process of 6-(2-ethoxymorpholino)-2-(4-methoxy-3-nitrobenzylsulfanyl)-9-methyl-9H-purine

There total 5 articles about 6-(2-ethoxymorpholino)-2-(4-methoxy-3-nitrobenzylsulfanyl)-9-methyl-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1253848-95-1
6-chloro-2-(4-methoxy-3-nitrobenzylsulfanyl)-9-methyl-9H-purine

: 2-ethoxymorpholine hydrochloride

: 1253848-25-7
6-(2-ethoxymorpholino)-2-(4-methoxy-3-nitrobenzylsulfanyl)-9-methyl-9H-purine

Guidance literature:: With triethylamine; In tetrahydrofuran; for 7h; Reflux;

Reference yield:

: 61010-34-2
3-nitro-4-methoxybenzyl bromide

: 1253848-25-7
6-(2-ethoxymorpholino)-2-(4-methoxy-3-nitrobenzylsulfanyl)-9-methyl-9H-purine

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / N,N-dimethyl-formamide / 3 h / 100 °C

2: trichlorophosphate; N,N-dimethyl-aniline / 1,4-dioxane / 2 h / 100 °C

3: sodium hydride / N,N-dimethyl-formamide / 0.08 h / Cooling with ice

4: triethylamine / tetrahydrofuran / 7 h / Reflux

With sodium hydride; N,N-dimethyl-aniline; triethylamine; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

: 2487-40-3
2-thioxanthine

: 1253848-25-7
6-(2-ethoxymorpholino)-2-(4-methoxy-3-nitrobenzylsulfanyl)-9-methyl-9H-purine

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / N,N-dimethyl-formamide / 3 h / 100 °C

2: trichlorophosphate; N,N-dimethyl-aniline / 1,4-dioxane / 2 h / 100 °C

3: sodium hydride / N,N-dimethyl-formamide / 0.08 h / Cooling with ice

4: triethylamine / tetrahydrofuran / 7 h / Reflux

With sodium hydride; N,N-dimethyl-aniline; triethylamine; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;