3-Oxo-4,4-diphenyl-pentanoic acid methoxycarbonylmethyl ester

Base Information

Chemical Name:3-Oxo-4,4-diphenyl-pentanoic acid methoxycarbonylmethyl ester
CAS No.:1026802-09-4
Molecular Formula:C₂₀H₂₀O₅
Molecular Weight:340.376
Hs Code.:

Synonyms:3-Oxo-4,4-diphenyl-pentanoic acid methoxycarbonylmethyl ester

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Chemical Property of 3-Oxo-4,4-diphenyl-pentanoic acid methoxycarbonylmethyl ester

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Technology Process of 3-Oxo-4,4-diphenyl-pentanoic acid methoxycarbonylmethyl ester

There total 3 articles about 3-Oxo-4,4-diphenyl-pentanoic acid methoxycarbonylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 22875-82-7
2,2-diphenylpropanal

: 149298-93-1
methyl (diazoacetoxy)acetate

: 1026802-09-4
3-Oxo-4,4-diphenyl-pentanoic acid methoxycarbonylmethyl ester

Guidance literature:: zirconium(IV) chloride; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/jo00081a035

Reference yield:

: 112641-77-7
2-methoxy-2-oxoethyl3-oxobutanoate

: 1026802-09-4
3-Oxo-4,4-diphenyl-pentanoic acid methoxycarbonylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: mesyl azide, triethylamine / tetrahydrofuran / 6 h / Ambient temperature

2: pyrrolidine / tetrahydrofuran

3: 65 percent / ZrCl₄ / CH₂Cl₂ / 1 h / 0 °C

With pyrrolidine; triethylamine; Methanesulfonyl azide; zirconium(IV) chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00081a035

Reference yield:

: 153791-43-6
2-Diazo-3-oxo-butyric acid methoxycarbonylmethyl ester

: 1026802-09-4
3-Oxo-4,4-diphenyl-pentanoic acid methoxycarbonylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyrrolidine / tetrahydrofuran

2: 65 percent / ZrCl₄ / CH₂Cl₂ / 1 h / 0 °C

With pyrrolidine; zirconium(IV) chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00081a035