Technology Process of C24H40INO5Si
There total 5 articles about C24H40INO5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
iodine; silver trifluoroacetate;
In
chloroform;
at -60 ℃;
for 120h;
Temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / water; 1,4-dioxane / -2 - 0 °C
2: N,N-dimethylformamide dineopentyl acetal / toluene / 3 h / Reflux
3: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C
4: silver trifluoroacetate; iodine / chloroform / 120 h / -60 °C
With
1H-imidazole; iodine; silver trifluoroacetate; triethylamine; N,N-dimethylformamide dineopentyl acetal;
In
1,4-dioxane; chloroform; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / water; 1,4-dioxane / -2 - 0 °C
2: N,N-dimethylformamide dineopentyl acetal / toluene / 3 h / Reflux
3: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C
4: silver trifluoroacetate; iodine / chloroform / 120 h / -60 °C
With
1H-imidazole; iodine; silver trifluoroacetate; triethylamine; N,N-dimethylformamide dineopentyl acetal;
In
1,4-dioxane; chloroform; water; N,N-dimethyl-formamide; toluene;