Technology Process of C23H28O3
There total 8 articles about C23H28O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 50 ℃;
for 7h;
regioselective reaction;
DOI:10.1016/j.tetlet.2012.04.030
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: di(n-butyl)tin oxide; triethylamine / dichloromethane / 20 °C
2.1: potassium carbonate / methanol / 1 h / 20 °C
3.1: magnesium / tetrahydrofuran
3.2: 3 h / -40 °C
4.1: sodium hydride / tetrahydrofuran / 12 h / 0 - 20 °C
5.1: methanol; toluene-4-sulfonic acid / 24 h / 20 °C
6.1: triethylamine / dichloromethane / 1 h / 20 °C
7.1: potassium carbonate / methanol / 2 h / 20 °C
8.1: lithium aluminium tetrahydride / tetrahydrofuran / 7 h / 50 °C
With
methanol; lithium aluminium tetrahydride; sodium hydride; di(n-butyl)tin oxide; potassium carbonate; toluene-4-sulfonic acid; magnesium; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tetlet.2012.04.030
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydride / tetrahydrofuran / 12 h / 0 - 20 °C
2: methanol; toluene-4-sulfonic acid / 24 h / 20 °C
3: triethylamine / dichloromethane / 1 h / 20 °C
4: potassium carbonate / methanol / 2 h / 20 °C
5: lithium aluminium tetrahydride / tetrahydrofuran / 7 h / 50 °C
With
methanol; lithium aluminium tetrahydride; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tetlet.2012.04.030
