2-[4-(4-chloro-phenyl)-piperazin-1-ylmethyl]-4-phenyl-pyrrolo[1,2-a]quinoxaline

Base Information

Chemical Name:2-[4-(4-chloro-phenyl)-piperazin-1-ylmethyl]-4-phenyl-pyrrolo[1,2-a]quinoxaline
CAS No.:326500-24-7
Molecular Formula:C₂₈H₂₅ClN₄
Molecular Weight:452.986
Hs Code.:

2-[4-(4-chloro-phenyl)-piperazin-1-ylmethyl]-4-phenyl-pyrrolo[1,2-<i>a</i>]quinoxaline

Synonyms:2-[4-(4-chloro-phenyl)-piperazin-1-ylmethyl]-4-phenyl-pyrrolo[1,2-a]quinoxaline

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Chemical Property of 2-[4-(4-chloro-phenyl)-piperazin-1-ylmethyl]-4-phenyl-pyrrolo[1,2-a]quinoxaline

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Technology Process of 2-[4-(4-chloro-phenyl)-piperazin-1-ylmethyl]-4-phenyl-pyrrolo[1,2-a]quinoxaline

There total 6 articles about 2-[4-(4-chloro-phenyl)-piperazin-1-ylmethyl]-4-phenyl-pyrrolo[1,2-a]quinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 38212-33-8
4-(4-chlorophenyl) piperazine

: 203513-49-9
4-phenylpyrrolo[1,2-a]quinoxaline-2-carboxaldehyde

: 326500-24-7
2-[4-(4-chloro-phenyl)-piperazin-1-ylmethyl]-4-phenyl-pyrrolo[1,2-a]quinoxaline

Guidance literature:: With sodium cyanoborohydride; In methanol; acetic acid; for 5h; pH=6.0; Heating;
DOI:10.1211/0022357001777522

Reference yield:

: 10130-23-1
2-methyl-3-phenylquinoxaline

: 326500-24-7
2-[4-(4-chloro-phenyl)-piperazin-1-ylmethyl]-4-phenyl-pyrrolo[1,2-a]quinoxaline

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / Heating

2: LiAlH₄ / tetrahydrofuran

3: MnO₂ / CHCl₃ / Heating

4: 74 percent / NaBH₃CN / methanol; acetic acid / 5 h / pH 6.0 / Heating

With manganese(IV) oxide; lithium aluminium tetrahydride; sodium cyanoborohydride; In tetrahydrofuran; methanol; ethanol; chloroform; acetic acid;
DOI:10.1211/0022357001777522

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 326500-24-7
2-[4-(4-chloro-phenyl)-piperazin-1-ylmethyl]-4-phenyl-pyrrolo[1,2-a]quinoxaline

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid

2: ethanol / Heating

3: LiAlH₄ / tetrahydrofuran

4: MnO₂ / CHCl₃ / Heating

5: 74 percent / NaBH₃CN / methanol; acetic acid / 5 h / pH 6.0 / Heating

With manganese(IV) oxide; lithium aluminium tetrahydride; sodium cyanoborohydride; In tetrahydrofuran; methanol; ethanol; chloroform; acetic acid;
DOI:10.1211/0022357001777522