Benzyl 4-(2-Methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-(2-nitroethyl)pyrrole-2-carboxylate

Base Information

Chemical Name:Benzyl 4-(2-Methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-(2-nitroethyl)pyrrole-2-carboxylate
CAS No.:101210-39-3
Molecular Formula:C₂₁H₂₄N₂O₈
Molecular Weight:432.43
Hs Code.:

Synonyms:Benzyl 4-(2-Methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-(2-nitroethyl)pyrrole-2-carboxylate

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Chemical Property of Benzyl 4-(2-Methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-(2-nitroethyl)pyrrole-2-carboxylate

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Technology Process of Benzyl 4-(2-Methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-(2-nitroethyl)pyrrole-2-carboxylate

There total 2 articles about Benzyl 4-(2-Methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-(2-nitroethyl)pyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 116683-95-5
(E)-Benzyl 4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-(2-nitroethenyl)pyrrole-2-carboxylate

: 101210-39-3
Benzyl 4-(2-Methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-(2-nitroethyl)pyrrole-2-carboxylate

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; for 0.0333333h;

Reference yield:

: 57529-24-5
benzyl 5-formyl-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrole-2-carboxylate

: 101210-39-3
Benzyl 4-(2-Methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-(2-nitroethyl)pyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / potassium acetate, methylamine hydrochloride / methanol / 2 h / 50 °C

2: 87 percent / NaBH₄ / CH₂Cl₂; methanol / 0.03 h

With sodium tetrahydroborate; methylamine hydrochloride; potassium acetate; In methanol; dichloromethane;

Reference yield:

: 101210-39-3
Benzyl 4-(2-Methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-(2-nitroethyl)pyrrole-2-carboxylate

: 101210-45-1
5-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-ylmethyl>-5-<5-<5-formyl-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrol-2-ylmethyl>pyrrolidi

Guidance literature:: Multi-step reaction with 6 steps

1: methylamine / acetic acid

2: borohydride

3: 1.) Triton B

4: Zn / acetic acid

6: tin(IV) chloride / CH₂Cl₂

With borohydride; N-benzyl-trimethylammonium hydroxide; methylamine; zinc; tin(IV) chloride; In dichloromethane; acetic acid;
DOI:10.1039/c39850001294