ent-4-hydroxy-3-methoxy-17-methyl-morphin-7-en-6-one-(2,4-dinitro-phenylhydrazone)

Base Information

• Chemical Name: ent-4-hydroxy-3-methoxy-17-methyl-morphin-7-en-6-one-(2,4-dinitro-phenylhydrazone)
• CAS No.: 123965-08-2
• Molecular Formula: C₂₄H₂₅N₅O₆
• Molecular Weight: 479.492
• Mol file: 123965-08-2.mol

Synonyms:ent-4-hydroxy-3-methoxy-17-methyl-morphin-7-en-6-one-(2,4-dinitro-phenylhydrazone)

Chemical Property of ent-4-hydroxy-3-methoxy-17-methyl-morphin-7-en-6-one-(2,4-dinitro-phenylhydrazone)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ent-4-hydroxy-3-methoxy-17-methyl-morphin-7-en-6-one-(2,4-dinitro-phenylhydrazone)

There total 1 articles about ent-4-hydroxy-3-methoxy-17-methyl-morphin-7-en-6-one-(2,4-dinitro-phenylhydrazone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ent-4,7ξ-dihydroxy-3-methoxy-17-methyl-morphinan-6-one → ent-4-hydroxy-3-methoxy-17-methyl-morphin-7-en-6-one-(2,4-dinitro-phenylhydrazone) (123965-08-2)

Guidance literature:

With acetic acid; und Behandeln des Reaktionsprodukts mit PCl₅ in Chloroform;

DOI:10.1016/S0020-1383(00)00169-8

Reference yield:

ent-4-hydroxy-3-methoxy-17-methyl-morphin-7-en-6-one-(2,4-dinitro-phenylhydrazone) (123965-08-2) → (±)-thebainone A (467-98-1,596-59-8,141901-27-1,141901-28-2)

Guidance literature:

Multi-step reaction with 2 steps

1: concentrated hydrochloric acid; acetone

2: Gewinnung

With hydrogenchloride; acetone;

DOI:10.1016/S0020-1383(00)00169-8

Downstream raw materials:

(±)-thebainone A