Dithiocarbonic acid S-((E)-2-methyl-3-phenyl-1-vinyl-allyl) ester S-prop-2-ynyl ester

Base Information

• Chemical Name: Dithiocarbonic acid S-((E)-2-methyl-3-phenyl-1-vinyl-allyl) ester S-prop-2-ynyl ester
• CAS No.: 185405-71-4
• Molecular Formula: C₁₆H₁₆OS₂
• Molecular Weight: 288.434

Synonyms:Dithiocarbonic acid S-((E)-2-methyl-3-phenyl-1-vinyl-allyl) ester S-prop-2-ynyl ester

Chemical Property of Dithiocarbonic acid S-((E)-2-methyl-3-phenyl-1-vinyl-allyl) ester S-prop-2-ynyl ester

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Technology Process of Dithiocarbonic acid S-((E)-2-methyl-3-phenyl-1-vinyl-allyl) ester S-prop-2-ynyl ester

There total 1 articles about Dithiocarbonic acid S-((E)-2-methyl-3-phenyl-1-vinyl-allyl) ester S-prop-2-ynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

Dithiocarbonic acid O-((2E,4E)-4-methyl-5-phenyl-penta-2,4-dienyl) ester S-prop-2-ynyl ester (185405-28-1) → Dithiocarbonic acid S-((E)-2-methyl-3-phenyl-1-vinyl-allyl) ester S-prop-2-ynyl ester (185405-71-4)

Guidance literature:

In benzene; for 2h; Heating;

DOI:10.1016/0040-4020(96)00853-8

Reference yield: 40.0%

Dithiocarbonic acid S-((E)-2-methyl-3-phenyl-1-vinyl-allyl) ester S-prop-2-ynyl ester (185405-71-4) → 5-methyl-6-phenyl-1,3,3a,6-tetrahydrobenzo[c]thiophene

Guidance literature:

In 1,2-dichloro-benzene; at 180 ℃; for 5h;

DOI:10.1016/0040-4020(96)00853-8

Reference yield: 28.0%

Dithiocarbonic acid S-((E)-2-methyl-3-phenyl-1-vinyl-allyl) ester S-prop-2-ynyl ester (185405-71-4) → ((1E,3E)-2-Methyl-5-prop-2-ynylsulfanyl-penta-1,3-dienyl)-benzene

Guidance literature:

With methylaluminum dichloride; In chloroform; at 0 ℃; for 5h;

DOI:10.1016/0040-4020(96)00853-8

upstream raw materials:

Dithiocarbonic acid O-((2E,4E)-4-methyl-5-phenyl-penta-2,4-dienyl) ester S-prop-2-ynyl ester

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