C₃₉H₅₂O₇Si

Base Information

• Chemical Name: C₃₉H₅₂O₇Si
• CAS No.: 1263144-32-6
• Molecular Formula: C₃₉H₅₂O₇Si
• Molecular Weight: 660.923
• Mol file: 1263144-32-6.mol

Synonyms:C₃₉H₅₂O₇Si

Chemical Property of C₃₉H₅₂O₇Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₃₉H₅₂O₇Si

There total 1 articles about C₃₉H₅₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C46H56O7Si → C39H52O7Si (1263144-32-6)

Guidance literature:

With pyridinium p-toluenesulfonate; In ethanol; at 20 ℃; for 18h;

DOI:10.1016/j.tet.2010.11.017

Reference yield:

C39H52O7Si (1263144-32-6) + t-butyldimethylsiyl triflate (69739-34-0) → C51H80O7Si3 (1263144-23-5)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 0.75h;

DOI:10.1016/j.tet.2010.11.017

Reference yield:

C39H52O7Si (1263144-32-6) → C49H78O6Si3 (1011784-38-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 0 °C

2.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.67 h / -78 °C

2.2: -78 °C

With 2,6-dimethylpyridine; diisobutylaluminium hydride; In hexane; dichloromethane;

DOI:10.1016/j.tet.2010.11.017

Downstream raw materials:

C₄₉H₇₈O₆Si₃

C₅₁H₈₀O₇Si₃