3-(2-methoxynaphthalen-1-yl)propynoic acid benzo[1,3]dioxol-5-ylbenzylamide

Base Information

Chemical Name:3-(2-methoxynaphthalen-1-yl)propynoic acid benzo[1,3]dioxol-5-ylbenzylamide
CAS No.:1308401-02-6
Molecular Formula:C₂₈H₂₁NO₄
Molecular Weight:435.479
Hs Code.:

Synonyms:3-(2-methoxynaphthalen-1-yl)propynoic acid benzo[1,3]dioxol-5-ylbenzylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-methoxynaphthalen-1-yl)propynoic acid benzo[1,3]dioxol-5-ylbenzylamide

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Technology Process of 3-(2-methoxynaphthalen-1-yl)propynoic acid benzo[1,3]dioxol-5-ylbenzylamide

There total 1 articles about 3-(2-methoxynaphthalen-1-yl)propynoic acid benzo[1,3]dioxol-5-ylbenzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 32932-20-0
N-(3,4-methylendioxyphenyl)-N-benzylamine

: 74877-61-5
3-(2-methoxynaphthalen-1-yl)propiolic acid

: 1308401-02-6
3-(2-methoxynaphthalen-1-yl)propynoic acid benzo[1,3]dioxol-5-ylbenzylamide

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 44.5h; Inert atmosphere;
DOI:10.1002/anie.201100152

Reference yield:

: 1308401-02-6
3-(2-methoxynaphthalen-1-yl)propynoic acid benzo[1,3]dioxol-5-ylbenzylamide

: (+)-5-benzyl-8-(2-methoxynaphthalen-1-yl)-5H-[1,3]dioxolo[4,5-g]quinolin-6-one

: (-)-5-benzyl-8-(2-methoxynaphthalen-1-yl)-5H-[1,3]dioxolo[4,5-g]quinolin-6-one

Guidance literature:: With tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); (S)-2,2'-bis[di(3,5-xylyl)phosphino]-5,5',6,6',7,7',8,8'-octahydro-1,1-binaphthyl; In 1,2-dichloro-ethane; at 20 ℃; for 72h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201100152

Reference yield:

: 1308401-02-6
3-(2-methoxynaphthalen-1-yl)propynoic acid benzo[1,3]dioxol-5-ylbenzylamide

: C₂₈H₂₁NO₄

: C₂₈H₂₁NO₄

Guidance literature:: With silver tetrafluoroborate; chloro(dimethylsulfide) gold(I); (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl; In 1,2-dichloro-ethane; at 20 ℃; for 40h; optical yield given as %ee; regioselective reaction; Inert atmosphere;
DOI:10.3762/bjoc.7.105