C₄₃H₅₂N₂O₂₁S₃

Base Information

Chemical Name:C₄₃H₅₂N₂O₂₁S₃
CAS No.:1383527-21-6
Molecular Formula:C₄₃H₅₂N₂O₂₁S₃
Molecular Weight:1029.08
Hs Code.:

C<sub>43</sub>H<sub>52</sub>N<sub>2</sub>O<sub>21</sub>S<sub>3</sub>

Synonyms:C₄₃H₅₂N₂O₂₁S₃

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Chemical Property of C₄₃H₅₂N₂O₂₁S₃

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Technology Process of C₄₃H₅₂N₂O₂₁S₃

There total 7 articles about C₄₃H₅₂N₂O₂₁S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3C₆H₁₅N*C₄₉H₆₆N₂O₂₂S₃Si

: 1383527-21-6
C₄₃H₅₂N₂O₂₁S₃

Guidance literature:: With magnesium bromide diethyl etherate; In diethyl ether; nitromethane; at 20 ℃; for 40h;
DOI:10.1016/j.carres.2012.04.010

Reference yield:

: 1383446-40-9
C₆₅H₈₂N₄O₁₃Si₂

: 1383527-21-6
C₄₃H₅₂N₂O₂₁S₃

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C

2: 1.3-propanedithiol; triethylamine / methanol / 40 h / 20 °C

3: sulfur trioxide pyridine complex; triethylamine / pyridine / 1 h / 70 °C / Microwave irradiation

4: magnesium bromide diethyl etherate / diethyl ether; nitromethane / 40 h / 20 °C

With 1.3-propanedithiol; magnesium bromide diethyl etherate; tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; triethylamine; In tetrahydrofuran; pyridine; methanol; diethyl ether; nitromethane;
DOI:10.1016/j.carres.2012.04.010

Reference yield:

: 1383446-52-3
C₆₁H₇₂N₂O₁₃Si

: 1383527-21-6
C₄₃H₅₂N₂O₂₁S₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide / 10 h / 55 °C

1.2: solid phase reaction

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 48 h / 20 °C

3.1: 1.3-propanedithiol; triethylamine / methanol / 40 h / 20 °C

4.1: sulfur trioxide pyridine complex; triethylamine / pyridine / 1 h / 70 °C / Microwave irradiation

5.1: magnesium bromide diethyl etherate / diethyl ether; nitromethane / 40 h / 20 °C

With 1.3-propanedithiol; magnesium bromide diethyl etherate; tetrabutyl ammonium fluoride; sulfur trioxide trimethylamine complex; sulfur trioxide pyridine complex; triethylamine; In tetrahydrofuran; pyridine; methanol; diethyl ether; nitromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2012.04.010