N'-(2-((trimethylsilyl)ethynyl)-benzylidene)-4-methylbenzenesulfonohydrazide

Base Information

Chemical Name:N'-(2-((trimethylsilyl)ethynyl)-benzylidene)-4-methylbenzenesulfonohydrazide
CAS No.:1361106-96-8
Molecular Formula:C₁₉H₂₂N₂O₂SSi
Molecular Weight:370.547
Hs Code.:

Synonyms:N'-(2-((trimethylsilyl)ethynyl)-benzylidene)-4-methylbenzenesulfonohydrazide

Suppliers and Price of N'-(2-((trimethylsilyl)ethynyl)-benzylidene)-4-methylbenzenesulfonohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N'-(2-((trimethylsilyl)ethynyl)-benzylidene)-4-methylbenzenesulfonohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N'-(2-((trimethylsilyl)ethynyl)-benzylidene)-4-methylbenzenesulfonohydrazide

There total 3 articles about N'-(2-((trimethylsilyl)ethynyl)-benzylidene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 77123-58-1
2-[2-(trimethylsilyl)ethynyl]benzaldehyde

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1361106-96-8
N'-(2-((trimethylsilyl)ethynyl)-benzylidene)-4-methylbenzenesulfonohydrazide

Guidance literature:: In methanol; at 20 ℃; for 2h;
DOI:10.1039/c2ob06611d

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 1361106-96-8
N'-(2-((trimethylsilyl)ethynyl)-benzylidene)-4-methylbenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 2 h / 100 °C / Microwave irradiation

2: methanol / 2 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1039/c2ob06611d

Reference yield:

: 1066-54-2
trimethylsilylacetylene

: 1361106-96-8
N'-(2-((trimethylsilyl)ethynyl)-benzylidene)-4-methylbenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 2 h / 100 °C / Microwave irradiation

2: methanol / 2 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1039/c2ob06611d