4-(methylbenzamido)-1,3,4,5-tetrahydro-5-hydroxy-α-methylenebenzindole-5-propionic acid γ-lactone

Base Information

Chemical Name:4-(methylbenzamido)-1,3,4,5-tetrahydro-5-hydroxy-α-methylenebenzindole-5-propionic acid γ-lactone
CAS No.:91424-45-2
Molecular Formula:C₂₃H₂₀N₂O₃
Molecular Weight:372.423
Hs Code.:

4-(methylbenzamido)-1,3,4,5-tetrahydro-5-hydroxy-α-methylenebenz<c,d>indole-5-propionic acid γ-lactone

Synonyms:4-(methylbenzamido)-1,3,4,5-tetrahydro-5-hydroxy-α-methylenebenzindole-5-propionic acid γ-lactone

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Chemical Property of 4-(methylbenzamido)-1,3,4,5-tetrahydro-5-hydroxy-α-methylenebenzindole-5-propionic acid γ-lactone

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Technology Process of 4-(methylbenzamido)-1,3,4,5-tetrahydro-5-hydroxy-α-methylenebenzindole-5-propionic acid γ-lactone

There total 4 articles about 4-(methylbenzamido)-1,3,4,5-tetrahydro-5-hydroxy-α-methylenebenzindole-5-propionic acid γ-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 91424-43-0
4-(methylbenzamido)-1,2,2a,3,4,5-hexahydro-5-hydroxy-α-methylenebenzindole-5-propionic acid γ-lactone

: 91424-45-2
4-(methylbenzamido)-1,3,4,5-tetrahydro-5-hydroxy-α-methylenebenzindole-5-propionic acid γ-lactone

Guidance literature:: With manganese(IV) oxide; In dichloromethane; Ambient temperature;
DOI:10.1021/jo00193a018

Reference yield:

: 91424-43-0
4-(methylbenzamido)-1,2,2a,3,4,5-hexahydro-5-hydroxy-α-methylenebenzindole-5-propionic acid γ-lactone

: 91424-45-2
4-(methylbenzamido)-1,3,4,5-tetrahydro-5-hydroxy-α-methylenebenzindole-5-propionic acid γ-lactone

Guidance literature:: With manganese(IV) oxide; In dichloromethane; Ambient temperature;
DOI:10.1021/jo00193a018

Reference yield:

: 88668-95-5
C₃₀H₂₆N₂O₄

: 91424-45-2
4-(methylbenzamido)-1,3,4,5-tetrahydro-5-hydroxy-α-methylenebenzindole-5-propionic acid γ-lactone

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / 1N HCl / methanol / 13 h / 70 °C

2: MnO₂ / CH₂Cl₂ / Ambient temperature

With hydrogenchloride; manganese(IV) oxide; In methanol; dichloromethane;
DOI:10.1021/jo00193a018