(3-(5-(2-(dimethylamino)ethoxy)-1H-indole-2-carbonyl)-5-nitro-2,3-dihydro-1H-benzo[e]indol-1yl)methyl phenylmethanesulfonate

Base Information

Chemical Name:(3-(5-(2-(dimethylamino)ethoxy)-1H-indole-2-carbonyl)-5-nitro-2,3-dihydro-1H-benzo[e]indol-1yl)methyl phenylmethanesulfonate
CAS No.:1333242-17-3
Molecular Formula:C₃₃H₃₂N₄O₇S
Molecular Weight:628.706
Hs Code.:

Synonyms:(3-(5-(2-(dimethylamino)ethoxy)-1H-indole-2-carbonyl)-5-nitro-2,3-dihydro-1H-benzo[e]indol-1yl)methyl phenylmethanesulfonate

Suppliers and Price of (3-(5-(2-(dimethylamino)ethoxy)-1H-indole-2-carbonyl)-5-nitro-2,3-dihydro-1H-benzo[e]indol-1yl)methyl phenylmethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3-(5-(2-(dimethylamino)ethoxy)-1H-indole-2-carbonyl)-5-nitro-2,3-dihydro-1H-benzo[e]indol-1yl)methyl phenylmethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3-(5-(2-(dimethylamino)ethoxy)-1H-indole-2-carbonyl)-5-nitro-2,3-dihydro-1H-benzo[e]indol-1yl)methyl phenylmethanesulfonate

There total 2 articles about (3-(5-(2-(dimethylamino)ethoxy)-1H-indole-2-carbonyl)-5-nitro-2,3-dihydro-1H-benzo[e]indol-1yl)methyl phenylmethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1333242-40-2
(5-(2-(dimethylamino)ethoxy)-1H-indol-2-yl)(1-(hydroxymethyl)-5-nitro-1H-benzo[e]indol-3(2H)-yl)methanone

: 1939-99-7
benzenesulfonyl chloride

: 1333242-17-3
(3-(5-(2-(dimethylamino)ethoxy)-1H-indole-2-carbonyl)-5-nitro-2,3-dihydro-1H-benzo[e]indol-1yl)methyl phenylmethanesulfonate

Guidance literature:: With pyridine; at 0 - 20 ℃; for 7h;
DOI:10.1016/j.bmc.2011.06.073

Reference yield:

: 193225-63-7
3-(tert-butoxycarbonyl)-1-(hydroxymethyl)-5-nitro-1,2-dihydro-3H-benzindole

: 5-<2-(dimethylamino)ethoxy>-1H-indole-2-carboxylic acid hydrochloride

: 1333242-17-3
(3-(5-(2-(dimethylamino)ethoxy)-1H-indole-2-carbonyl)-5-nitro-2,3-dihydro-1H-benzo[e]indol-1yl)methyl phenylmethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / 1,4-dioxane / 10 - 20 °C

1.2: 3 h / 20 °C

2.1: pyridine / 7 h / 0 - 20 °C

With pyridine; hydrogenchloride; In 1,4-dioxane;
DOI:10.1016/j.bmc.2011.06.073