N,N',N''-trihexadecyl-3,3',3''-[(4-methoxycarbonylphenyl-carbonylamino)methanetriyl]tripropanamide

Base Information

Chemical Name:N,N',N''-trihexadecyl-3,3',3''-[(4-methoxycarbonylphenyl-carbonylamino)methanetriyl]tripropanamide
CAS No.:926649-24-3
Molecular Formula:C₆₇H₁₂₂N₄O₆
Molecular Weight:1079.73
Hs Code.:

Synonyms:N,N',N''-trihexadecyl-3,3',3''-[(4-methoxycarbonylphenyl-carbonylamino)methanetriyl]tripropanamide

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Chemical Property of N,N',N''-trihexadecyl-3,3',3''-[(4-methoxycarbonylphenyl-carbonylamino)methanetriyl]tripropanamide

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Technology Process of N,N',N''-trihexadecyl-3,3',3''-[(4-methoxycarbonylphenyl-carbonylamino)methanetriyl]tripropanamide

There total 4 articles about N,N',N''-trihexadecyl-3,3',3''-[(4-methoxycarbonylphenyl-carbonylamino)methanetriyl]tripropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 926649-21-0
N,N',N''-trihexadecyl-3,3',3''-(1-aminomethanetriyl)tripropanamide

: 1679-64-7
Monomethyl terephthalate

: 926649-24-3
N,N',N''-trihexadecyl-3,3',3''-[(4-methoxycarbonylphenyl-carbonylamino)methanetriyl]tripropanamide

Guidance literature:: Monomethyl terephthalate; With thionyl chloride; N,N-dimethyl-formamide; Heating;

N,N',N''-trihexadecyl-3,3',3''-(1-aminomethanetriyl)tripropanamide; With triethylamine; In tetrahydrofuran; at 40 ℃; Further stages.;
DOI:10.1039/b609645j

Reference yield:

: 926649-19-6
N,N',N''-trihexadecyl-3,3',3''-(1-nitromethanetriyl)tripropanamide

: 926649-24-3
N,N',N''-trihexadecyl-3,3',3''-[(4-methoxycarbonylphenyl-carbonylamino)methanetriyl]tripropanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 83 percent / H₂ / Raney-Ni / ethanol / 24 h / 60 °C / 2625.26 Torr

2.1: SOCl₂; DMF / Heating

2.2: 76 percent / Et₃N / tetrahydrofuran / 40 °C

With thionyl chloride; hydrogen; N,N-dimethyl-formamide; nickel; In ethanol;
DOI:10.1039/b609645j

Reference yield:

: 143-27-1
hexadecylamine

: 926649-24-3
N,N',N''-trihexadecyl-3,3',3''-[(4-methoxycarbonylphenyl-carbonylamino)methanetriyl]tripropanamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: SOCl; DMF / Heating

1.2: 66 percent / Et₃N / tetrahydrofuran / 96 h / 40 °C

2.1: 83 percent / H₂ / Raney-Ni / ethanol / 24 h / 60 °C / 2625.26 Torr

3.1: SOCl₂; DMF / Heating

3.2: 76 percent / Et₃N / tetrahydrofuran / 40 °C

With thionyl chloride; hydrogen; N,N-dimethyl-formamide; nickel; In ethanol;
DOI:10.1039/b609645j