Technology Process of N,N',N''-trihexadecyl-3,3',3''-[(4-methoxycarbonylphenyl-carbonylamino)methanetriyl]tripropanamide
There total 4 articles about N,N',N''-trihexadecyl-3,3',3''-[(4-methoxycarbonylphenyl-carbonylamino)methanetriyl]tripropanamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Monomethyl terephthalate;
With
thionyl chloride; N,N-dimethyl-formamide;
Heating;
N,N',N''-trihexadecyl-3,3',3''-(1-aminomethanetriyl)tripropanamide;
With
triethylamine;
In
tetrahydrofuran;
at 40 ℃;
Further stages.;
DOI:10.1039/b609645j
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 83 percent / H2 / Raney-Ni / ethanol / 24 h / 60 °C / 2625.26 Torr
2.1: SOCl2; DMF / Heating
2.2: 76 percent / Et3N / tetrahydrofuran / 40 °C
With
thionyl chloride; hydrogen; N,N-dimethyl-formamide;
nickel;
In
ethanol;
DOI:10.1039/b609645j
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: SOCl; DMF / Heating
1.2: 66 percent / Et3N / tetrahydrofuran / 96 h / 40 °C
2.1: 83 percent / H2 / Raney-Ni / ethanol / 24 h / 60 °C / 2625.26 Torr
3.1: SOCl2; DMF / Heating
3.2: 76 percent / Et3N / tetrahydrofuran / 40 °C
With
thionyl chloride; hydrogen; N,N-dimethyl-formamide;
nickel;
In
ethanol;
DOI:10.1039/b609645j
