C₃₄H₆₅BrO₆Si₃

Base Information

Chemical Name:C₃₄H₆₅BrO₆Si₃
CAS No.:1351619-36-7
Molecular Formula:C₃₄H₆₅BrO₆Si₃
Molecular Weight:734.047
Hs Code.:

C<sub>34</sub>H<sub>65</sub>BrO<sub>6</sub>Si<sub>3</sub>

Synonyms:C₃₄H₆₅BrO₆Si₃

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Chemical Property of C₃₄H₆₅BrO₆Si₃

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Technology Process of C₃₄H₆₅BrO₆Si₃

There total 7 articles about C₃₄H₆₅BrO₆Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1351619-42-5
C₂₀H₃₁BrO₆

: 69739-34-0
t-butyldimethylsiyl triflate

: 1351619-36-7
C₃₄H₆₅BrO₆Si₃

Guidance literature:: C₂₀H₃₁BrO₆; t-butyldimethylsiyl triflate; With 2,6-dimethylpyridine; In dichloromethane; at 0 - 20 ℃; for 22h; Inert atmosphere;

With water; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; for 2h;
DOI:10.1016/j.tet.2011.09.058

Reference yield:

: 1351619-56-1
C₂₂H₃₃BrO₇

: 1351619-36-7
C₃₄H₆₅BrO₆Si₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium triethylborohydride / tetrahydrofuran / 0 - 20 °C

2.1: 2,6-dimethylpyridine / dichloromethane / 22 h / 0 - 20 °C / Inert atmosphere

2.2: 2 h

With 2,6-dimethylpyridine; lithium triethylborohydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2011.09.058

Reference yield:

: 1351619-40-3
C₂₂H₂₉BrO₇

: 1351619-36-7
C₃₄H₆₅BrO₆Si₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: RuBr₂{(R)-2,2'-bis(diphenylphosphino)-1,1'-dinaphthyl}; hydrogen / ethanol / 44 h / 45 °C / 30003 Torr / High-pressure bomb

2.1: lithium triethylborohydride / tetrahydrofuran / 0 - 20 °C

3.1: 2,6-dimethylpyridine / dichloromethane / 22 h / 0 - 20 °C / Inert atmosphere

3.2: 2 h

With 2,6-dimethylpyridine; RuBr₂{(R)-2,2'-bis(diphenylphosphino)-1,1'-dinaphthyl}; hydrogen; lithium triethylborohydride; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.tet.2011.09.058