(C₆H₅CC₄H₂N)3CC₄H₂NC₆H₄NHCOCH₂BrZn

Base Information

Chemical Name:(C₆H₅CC₄H₂N)3CC₄H₂NC₆H₄NHCOCH₂BrZn
CAS No.:158335-26-3
Molecular Formula:C₄₆H₃₀BrN₅OZn
Molecular Weight:814.071
Hs Code.:

(C<sub>6</sub>H<sub>5</sub>CC<sub>4</sub>H<sub>2</sub>N)3CC<sub>4</sub>H<sub>2</sub>NC<sub>6</sub>H<sub>4</sub>NHCOCH<sub>2</sub>BrZn

Synonyms:(C₆H₅CC₄H₂N)3CC₄H₂NC₆H₄NHCOCH₂BrZn

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Chemical Property of (C₆H₅CC₄H₂N)3CC₄H₂NC₆H₄NHCOCH₂BrZn

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Technology Process of (C₆H₅CC₄H₂N)3CC₄H₂NC₆H₄NHCOCH₂BrZn

There total 1 articles about (C₆H₅CC₄H₂N)3CC₄H₂NC₆H₄NHCOCH₂BrZn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: meso-(o-bromoacetamidophenyl)triphenylporphyrine

: 5970-45-6
zinc(II) acetate dihydrate

: 158335-26-3
(C₆H₅CC₄H₂N)3CC₄H₂NC₆H₄NHCOCH₂BrZn

Guidance literature:: With sodium acetate; In methanol; dichloromethane; 1.2 equivalents of the zinc acetate, sodium acetate and the solvent mixture were heated to reflux for 30 min;; solvent removal in vacuo; dilution of the residue in CH2Cl2, washing of the solution with water; drying of the organic phase; solvent removal; recrystn. from CH2Cl2/heptane;;

Reference yield: 70.0%

: 295-37-4
1,4,8,11-Tetraazacyclotetradecane

: 158335-26-3
(C₆H₅CC₄H₂N)3CC₄H₂NC₆H₄NHCOCH₂BrZn

: 158335-29-6
(C₆H₅CC₄H₂NH)2(C₆H₅CC₄H₂N)CC₄H₂NC₆H₄NHCOCH₂N(CH₂)3N(CH₂)2NH(CH₂)3N(CH₂)2Zn

Guidance literature:: In chloroform; stirring for 24 h;; washing with aqueous KOH, then to neutral with water; drying the organic layer over MgSO4; solvent removal; column chromy. (Al2O3, CH2Cl2/CH3OH);