C₁₈H₂₃N₃O₂

Base Information

Chemical Name:C₁₈H₂₃N₃O₂
CAS No.:1415726-57-6
Molecular Formula:C₁₈H₂₃N₃O₂
Molecular Weight:313.4
Hs Code.:

C<sub>18</sub>H<sub>23</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:C₁₈H₂₃N₃O₂

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Chemical Property of C₁₈H₂₃N₃O₂

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Technology Process of C₁₈H₂₃N₃O₂

There total 5 articles about C₁₈H₂₃N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₂₁N₃O₂

: 1415726-57-6
C₁₈H₂₃N₃O₂

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 1h;
DOI:10.1016/j.jorganchem.2012.08.037

Reference yield:

: 132393-21-6
tert-butyl 3-methyl-1-oxo-1-(pyridin-2-ylmethylamino)butan-2-ylcarbamate

: 1415726-57-6
C₁₈H₂₃N₃O₂

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C

2: sodium sulfate; potassium carbonate / ethanol / 2 h / 20 °C

3: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

With sodium tetrahydroborate; potassium carbonate; sodium sulfate; trifluoroacetic acid; In methanol; ethanol; dichloromethane;
DOI:10.1016/j.jorganchem.2012.08.037

Reference yield:

: 72-18-4,25609-85-2,7004-03-7,921-10-8
L-valine

: 1415726-57-6
C₁₈H₂₃N₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / tetrahydrofuran; water / 0 - 20 °C

1.2: 12 h / 0 - 20 °C

2.1: dicyclohexyl-carbodiimide / dichloromethane / 1 h / 0 °C

2.2: 12 h / 0 - 20 °C

3.1: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C

4.1: sodium sulfate; potassium carbonate / ethanol / 2 h / 20 °C

5.1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

With sodium tetrahydroborate; potassium carbonate; sodium sulfate; dicyclohexyl-carbodiimide; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water;
DOI:10.1016/j.jorganchem.2012.08.037