N-(3-((2S,4S,5S,7S)-5-amino-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methylnonanamido)-2,2-dimethylpropyl)-4-methoxybenzamide

Base Information

Chemical Name:N-(3-((2S,4S,5S,7S)-5-amino-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methylnonanamido)-2,2-dimethylpropyl)-4-methoxybenzamide
CAS No.:1321622-30-3
Molecular Formula:C₃₈H₆₁N₃O₇
Molecular Weight:671.918
Hs Code.:

N-(3-((2S,4S,5S,7S)-5-amino-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methylnonanamido)-2,2-dimethylpropyl)-4-methoxybenzamide

Synonyms:N-(3-((2S,4S,5S,7S)-5-amino-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methylnonanamido)-2,2-dimethylpropyl)-4-methoxybenzamide

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Chemical Property of N-(3-((2S,4S,5S,7S)-5-amino-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methylnonanamido)-2,2-dimethylpropyl)-4-methoxybenzamide

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Technology Process of N-(3-((2S,4S,5S,7S)-5-amino-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methylnonanamido)-2,2-dimethylpropyl)-4-methoxybenzamide

There total 8 articles about N-(3-((2S,4S,5S,7S)-5-amino-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methylnonanamido)-2,2-dimethylpropyl)-4-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1321622-48-3
N-(3-((2S,4S,5S,7S)-5-azido-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methyl nonanamido)-2,2-dimethylpropyl)-4-methoxybenzamide

: 1321622-30-3
N-(3-((2S,4S,5S,7S)-5-amino-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methylnonanamido)-2,2-dimethylpropyl)-4-methoxybenzamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; ethanolamine; In tert-butyl methyl ether; at 25 ℃;
DOI:10.1016/j.bmc.2011.05.059

Reference yield:

: 1321622-82-5
N-(3-azido-2,2-dimethylpropyl)-4-methoxybenzamide

: 1321622-30-3
N-(3-((2S,4S,5S,7S)-5-amino-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methylnonanamido)-2,2-dimethylpropyl)-4-methoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 25 °C

2: 2-hydroxypyridin; triethylamine / 65 °C

3: palladium 10% on activated carbon; hydrogen; ethanolamine / tert-butyl methyl ether / 25 °C

With 2-hydroxypyridin; palladium 10% on activated carbon; hydrogen; ethanolamine; triethylamine; In methanol; tert-butyl methyl ether;
DOI:10.1016/j.bmc.2011.05.059

Reference yield:

: 111992-61-1
2-(3-bromo-2, 2-dimethylpropyl)-2,3-dihydro-1H-isoindole-1,3-dione

: 1321622-30-3
N-(3-((2S,4S,5S,7S)-5-amino-4-hydroxy-2-isopropyl-7-(4-methoxy-3-(3-methoxypropoxy)benzyl)-8-methylnonanamido)-2,2-dimethylpropyl)-4-methoxybenzamide

Guidance literature:: Multi-step reaction with 6 steps

1: sodium azide / N,N-dimethyl-formamide / 8 h / 100 °C

2: hydrazine hydrate / ethanol / 4 h / 80 °C

3: triethylamine / dichloromethane / 0 - 25 °C

4: palladium 10% on activated carbon; hydrogen / methanol / 25 °C

5: 2-hydroxypyridin; triethylamine / 65 °C

6: palladium 10% on activated carbon; hydrogen; ethanolamine / tert-butyl methyl ether / 25 °C

With 2-hydroxypyridin; sodium azide; palladium 10% on activated carbon; hydrogen; hydrazine hydrate; ethanolamine; triethylamine; In methanol; ethanol; dichloromethane; tert-butyl methyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.05.059